3-[bis(pentafluorophenyl)boryl]-2,5-bis(trimethylsilyl)-1,1-diphenylsilole

Base Information

• Chemical Name: 3-[bis(pentafluorophenyl)boryl]-2,5-bis(trimethylsilyl)-1,1-diphenylsilole
• CAS No.: 1228942-33-3
• Molecular Formula: C₃₄H₂₉BF₁₀Si₃
• Molecular Weight: 722.656

Synonyms:3-[bis(pentafluorophenyl)boryl]-2,5-bis(trimethylsilyl)-1,1-diphenylsilole

Chemical Property of 3-[bis(pentafluorophenyl)boryl]-2,5-bis(trimethylsilyl)-1,1-diphenylsilole

Chemical Property:

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Technology Process of 3-[bis(pentafluorophenyl)boryl]-2,5-bis(trimethylsilyl)-1,1-diphenylsilole

There total 4 articles about 3-[bis(pentafluorophenyl)boryl]-2,5-bis(trimethylsilyl)-1,1-diphenylsilole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

bis((trimethylsilyl)ethynyl)diphenylsilane (25284-31-5) + bis(pentafluorophenyl)borohydride (165612-94-2) → 3-[bis(pentafluorophenyl)boryl]-2,5-bis(trimethylsilyl)-1,1-diphenylsilole (1228942-33-3)

Guidance literature:

In toluene; at 20 ℃; Inert atmosphere;

DOI:10.1039/b927221f

Reference yield:

Si(C6H5)2(C2HSi(CH3)3)(CSi(CH3)3)CB(C6F5)2 (1292785-45-5) → 3-[bis(pentafluorophenyl)boryl]-2,5-bis(trimethylsilyl)-1,1-diphenylsilole (1228942-33-3)

Guidance literature:

In ⁽²⁾H₈-toluene; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.jorganchem.2010.09.024

Reference yield:

bis((trimethylsilyl)ethynyl)diphenylsilane (25284-31-5) → 3-[bis(pentafluorophenyl)boryl]-2,5-bis(trimethylsilyl)-1,1-diphenylsilole (1228942-33-3)

Guidance literature:

In toluene; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.jorganchem.2010.09.024

upstream raw materials:

bis((trimethylsilyl)ethynyl)diphenylsilane

bis(pentafluorophenyl)borohydride

Si(C₆H₅)2(C₂HSi(CH₃)3)(CSi(CH₃)3)CB(C₆F₅)2

Downstream raw materials:

5-[bis(pentafluorophenyl)boryl]-2,3-bis(trimethylsilyl)-1,1-diphenylsilole

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