3-(Bromomethyl)-4-chlorophenyl methanesulfonate

Base Information

Chemical Name:3-(Bromomethyl)-4-chlorophenyl methanesulfonate
CAS No.:335160-95-7
Molecular Formula:C₈H₈BrClO₃S
Molecular Weight:299.573
Hs Code.:
DSSTox Substance ID:DTXSID501213124
Nikkaji Number:J1.613.101F

Synonyms:3-(bromomethyl)-4-chlorophenyl methanesulfonate;SCHEMBL6901293;IRZDKLGHMZSCEG-UHFFFAOYSA-N;DTXSID501213124;335160-95-7;Phenol, 3-(bromomethyl)-4-chloro-, 1-methanesulfonate

Suppliers and Price of 3-(Bromomethyl)-4-chlorophenyl methanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(Bromomethyl)-4-chlorophenyl methanesulfonate

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:297.90661
Heavy Atom Count:14
Complexity:275

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CS(=O)(=O)OC1=CC(=C(C=C1)Cl)CBr

Technology Process of 3-(Bromomethyl)-4-chlorophenyl methanesulfonate

There total 3 articles about 3-(Bromomethyl)-4-chlorophenyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 90555-52-5
4'-chloro-3'-methylphenyl methanesulfonate

: 335160-95-7
3-(bromomethyl)-4-chloro-1-phenyl methanesulfonate

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 80 ℃; for 14h;
DOI:10.1021/ol015504w

Reference yield:

: 34241-39-9
azobisisobutyronitrile

: 90555-52-5
4'-chloro-3'-methylphenyl methanesulfonate

: 335160-95-7
3-(bromomethyl)-4-chloro-1-phenyl methanesulfonate

Guidance literature:: With N-Bromosuccinimide; In tetrachloromethane; hexane; ethyl acetate;

Reference yield:

: 59-50-7
4-Chloro-3-methylphenol

: 335160-95-7
3-(bromomethyl)-4-chloro-1-phenyl methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 0 °C

2: NBS; AIBN / CCl₄ / Heating

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); triethylamine; In tetrachloromethane; dichloromethane;
DOI:10.1016/j.bmcl.2003.11.051