methanol adduct of α-phenyl-N-t-butylnitrone

Base Information

• Chemical Name: methanol adduct of α-phenyl-N-t-butylnitrone
• CAS No.: 34280-33-6
• Molecular Formula: C₁₂H₁₈NO₂
• Molecular Weight: 208.28
• Mol file: 34280-33-6.mol

Synonyms:methanol adduct of α-phenyl-N-t-butylnitrone

Chemical Property of methanol adduct of α-phenyl-N-t-butylnitrone

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of methanol adduct of α-phenyl-N-t-butylnitrone

There total 4 articles about methanol adduct of α-phenyl-N-t-butylnitrone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + t-butylnitrite (917-95-3) → methanol adduct of α-phenyl-N-t-butylnitrone (34280-33-6)

Guidance literature:

With terephthalonitrile; water; In acetonitrile; for 2h; UV-irradiation;

DOI:10.1002/jccs.200100144

Reference yield:

methanol (67-56-1) + N-tert-butyl-α-phenylnitrone (3376-24-7,68315-30-0) → methanol adduct of α-phenyl-N-t-butylnitrone (34280-33-6)

Guidance literature:

With photoexcited benzophenone;

Reference yield:

methanol (67-56-1) + (Z)-N-benzylidene-2-methylpropan-2-amine oxide (3376-24-7,52392-70-8,85225-53-2,68315-30-0) → methanol adduct of α-phenyl-N-t-butylnitrone (34280-33-6)

Guidance literature:

With potassium hexachloropalatinate(IV); 18-crown-6 ether; at 20 ℃; Product distribution; Irradiation;

DOI:10.1039/DT9890001237

upstream raw materials:

methanol

(Z)-N-benzylidene-2-methylpropan-2-amine oxide

N-tert-butyl-α-phenylnitrone

styrene