(1R,2R)-N,N'-bis(2,4,6-triisopropylbenzenesulfonyl)-cyclohexane-1,2-diamine

Base Information

Chemical Name:(1R,2R)-N,N'-bis(2,4,6-triisopropylbenzenesulfonyl)-cyclohexane-1,2-diamine
CAS No.:143585-49-3
Molecular Formula:C₃₆H₅₈N₂O₄S₂
Molecular Weight:647
Hs Code.:

Synonyms:(1R,2R)-N,N'-bis(2,4,6-triisopropylbenzenesulfonyl)-cyclohexane-1,2-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R)-N,N'-bis(2,4,6-triisopropylbenzenesulfonyl)-cyclohexane-1,2-diamine

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Technology Process of (1R,2R)-N,N'-bis(2,4,6-triisopropylbenzenesulfonyl)-cyclohexane-1,2-diamine

There total 3 articles about (1R,2R)-N,N'-bis(2,4,6-triisopropylbenzenesulfonyl)-cyclohexane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 20439-47-8
(1R,2R)-1,2-diaminocyclohexane

: 143585-49-3
(1R,2R)-N,N'-bis(2,4,6-triisopropylbenzenesulfonyl)-cyclohexane-1,2-diamine

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/adsc.200700084

Reference yield: 84.0%

: 63877-57-6
2,4,6-tri(iso-propyl)benzenesulfonic acid

: 20439-47-8
(1R,2R)-1,2-diaminocyclohexane

: 143585-49-3
(1R,2R)-N,N'-bis(2,4,6-triisopropylbenzenesulfonyl)-cyclohexane-1,2-diamine

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c5ra18871g

Reference yield: 58.0%

: 591-87-7
Allyl acetate

: trans-N,N'-bis-(2,4,6-triisopropyl)phenylsulfonyl-1,2-diaminocyclohexane

: 143585-49-3
(1R,2R)-N,N'-bis(2,4,6-triisopropylbenzenesulfonyl)-cyclohexane-1,2-diamine

: (1S,2S)-N,N'-bis-(2,4,6-triisopropyl)phenylsulfonyl-1,2-diaminocyclohexane

: C₃₉H₆₂N₂O₄S₂

Guidance literature:: With bis(η3-allyl-μ-chloropalladium(II)); potassium tert-butylate; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane; In 1,4-dioxane; toluene; at -15 - -10 ℃; for 10h; Title compound not separated from byproducts;
DOI:10.1021/ol048498n