N,N'-bis(4-methoxy-2,6-diisopropylphenyl)-1,4-diazabutadiene

Base Information

• Chemical Name: N,N'-bis(4-methoxy-2,6-diisopropylphenyl)-1,4-diazabutadiene
• CAS No.: 1619907-20-8
• Molecular Formula: C₂₈H₄₀N₂O₂
• Molecular Weight: 436.638
• Mol file: 1619907-20-8.mol

Synonyms:N,N'-bis(4-methoxy-2,6-diisopropylphenyl)-1,4-diazabutadiene

Chemical Property of N,N'-bis(4-methoxy-2,6-diisopropylphenyl)-1,4-diazabutadiene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-bis(4-methoxy-2,6-diisopropylphenyl)-1,4-diazabutadiene

There total 3 articles about N,N'-bis(4-methoxy-2,6-diisopropylphenyl)-1,4-diazabutadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

Glyoxal (131543-46-9,107-22-2) + 4-(methoxy)-2,6-diisopropylaniline (1394159-51-3) → N,N'-bis(4-methoxy-2,6-diisopropylphenyl)-1,4-diazabutadiene (1619907-20-8)

Guidance literature:

With formic acid; In methanol; water; at 20 ℃; for 2h;

Reference yield:

2,6-diisopropylbenzenamine (24544-04-5) → N,N'-bis(4-methoxy-2,6-diisopropylphenyl)-1,4-diazabutadiene (1619907-20-8)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium carbonate; iodine / cyclohexane; water / 11 h / 20 °C

2: formic acid / water; methanol

3: copper(l) iodide; 1,10-Phenanthroline; caesium carbonate / 10 h / Sealed tube; Heating

4: formic acid / water; methanol / 20 °C

With copper(l) iodide; formic acid; 1,10-Phenanthroline; iodine; sodium carbonate; caesium carbonate; In methanol; cyclohexane; water;

DOI:10.1055/s-0033-1340105

Reference yield:

4-iodo-2,6-diisopropylaniline (140411-20-7) → N,N'-bis(4-methoxy-2,6-diisopropylphenyl)-1,4-diazabutadiene (1619907-20-8)

Guidance literature:

Multi-step reaction with 3 steps

1: formic acid / water; methanol

2: copper(l) iodide; 1,10-Phenanthroline; caesium carbonate / 10 h / Sealed tube; Heating

3: formic acid / water; methanol / 20 °C

With copper(l) iodide; formic acid; 1,10-Phenanthroline; caesium carbonate; In methanol; water;

DOI:10.1055/s-0033-1340105

upstream raw materials:

Glyoxal

4-(methoxy)-2,6-diisopropylaniline

2,6-diisopropylbenzenamine

4-iodo-2,6-diisopropylaniline

Downstream raw materials:

N,N'-bis(4-methoxy-2,6-diisopropylphenylamino)ethane-1,2-diamine

1,3-bis-(4-methoxy-2,6-diisopropylphenyl)-4,5-dihydroimidazolinium chloride

[1,3-bis(4-methoxy-2,6-diisopropyl)phenyl]imidazolium chloride