C₆H₅C(OH)(C₆H₃)(C₁₀H₅)(OCH₃)4

Base Information

• Chemical Name: C₆H₅C(OH)(C₆H₃)(C₁₀H₅)(OCH₃)4
• CAS No.: 915706-56-8
• Molecular Formula: C₂₇H₂₆O₅
• Molecular Weight: 430.5
• Mol file: 915706-56-8.mol

Synonyms:C₆H₅C(OH)(C₆H₃)(C₁₀H₅)(OCH₃)4

Chemical Property of C₆H₅C(OH)(C₆H₃)(C₁₀H₅)(OCH₃)4

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆H₅C(OH)(C₆H₃)(C₁₀H₅)(OCH₃)4

There total 1 articles about C₆H₅C(OH)(C₆H₃)(C₁₀H₅)(OCH₃)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

1,6-dimethoxynaphthalene (3900-49-0) + 2,4-dimethoxybenzophenone (3555-84-8) → C6H5C(OH)(C6H3)(C10H5)(OCH3)4 (915706-56-8) + C6H5C(OH)(C6H3)(C10H5)(OCH3)4 (915706-57-9) + C6H5C(OH)(C6H3)(C10H5)(OCH3)3(OH)

Guidance literature:

1,6-dimethoxynaphthalene; With n-butyllithium;

2,4-dimethoxybenzophenone; In tetrahydrofuran; at -78 - 20 ℃; Further stages.;

DOI:10.1021/ja0632207

Reference yield: 100.0%

C6H5C(OH)(C6H3)(C10H5)(OCH3)4 (915706-56-8) → C24H16O3 (915706-60-4)

Guidance literature:

With boron tribromide;

Reference yield:

C6H5C(OH)(C6H3)(C10H5)(OCH3)4 (915706-56-8) → C23H13O3BBr2

Guidance literature:

Multi-step reaction with 2 steps

1.1: BBr₃ / CH₂Cl₂ / 50 °C

1.2: 99 percent / H₂O / CH₂Cl₂

2.1: BBr₃ / CH₂Cl₂ / -78 - 20 °C

With boron tribromide; In dichloromethane;

DOI:10.1021/ja0632207

upstream raw materials:

1,6-dimethoxynaphthalene

2,4-dimethoxybenzophenone

Downstream raw materials:

C₂₄H₁₆O₃

C₂₃H₁₄O₃

Refernces

• 1、 Yang, Youjun,Lowry, Mark,Schowalter, Corin M.,Fakayode, Sayo O.,Escobedo, Jorge O.,Xu, Xiangyang,Zhang, Huating,Jensen, Timothy J.,Fronczek, Frank R.,Warner, Isiah M.,Strongin, Robert M.. "An organic white light-emitting fluorophore". . p. 14081 - 14092. Retrieved 2008/02/10.