N-{6-[({[(1-methyl-1H-1,2,4-triazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}hexanamide

Base Information

Chemical Name:N-{6-[({[(1-methyl-1H-1,2,4-triazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}hexanamide
CAS No.:1192573-22-0
Molecular Formula:C₂₂H₂₆N₆O₂
Molecular Weight:406.487
Hs Code.:

Synonyms:N-{6-[({[(1-methyl-1H-1,2,4-triazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}hexanamide

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Chemical Property of N-{6-[({[(1-methyl-1H-1,2,4-triazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}hexanamide

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Technology Process of N-{6-[({[(1-methyl-1H-1,2,4-triazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}hexanamide

There total 5 articles about N-{6-[({[(1-methyl-1H-1,2,4-triazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}hexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1192572-98-7
6-[({[(1-methyl-1H-1,2,4-triazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-amine

: 142-61-0
Hexanoyl chloride

: 1192573-22-0
N-{6-[({[(1-methyl-1H-1,2,4-triazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}hexanamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 4h;

Reference yield:

: 77375-17-8
2-methyl-1,2,4-triazol-3-yl phenyl ketone

: 1192573-22-0
N-{6-[({[(1-methyl-1H-1,2,4-triazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}hexanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine; hydroxylamine hydrochloride / 50 °C

2.1: caesium carbonate / potassium iodide / acetonitrile / 0.08 h

2.2: 4 h / 20 °C

3.1: hydrazine hydrate / tetrahydrofuran / 20 °C

4.1: triethylamine / dichloromethane / 4 h / 20 °C

With pyridine; hydroxylamine hydrochloride; caesium carbonate; hydrazine hydrate; triethylamine; potassium iodide; In tetrahydrofuran; dichloromethane; acetonitrile;

Reference yield:

: 98-88-4
benzoyl chloride

: 1192573-22-0
N-{6-[({[(1-methyl-1H-1,2,4-triazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}hexanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / acetonitrile / -5 - 20 °C

2.1: pyridine; hydroxylamine hydrochloride / 50 °C

3.1: caesium carbonate / potassium iodide / acetonitrile / 0.08 h

3.2: 4 h / 20 °C

4.1: hydrazine hydrate / tetrahydrofuran / 20 °C

5.1: triethylamine / dichloromethane / 4 h / 20 °C

With pyridine; hydroxylamine hydrochloride; caesium carbonate; hydrazine hydrate; triethylamine; potassium iodide; In tetrahydrofuran; dichloromethane; acetonitrile;