C₂₁H₃₇NO₃Si

Base Information Edit

Chemical Name:C₂₁H₃₇NO₃Si
CAS No.:1072091-11-2
Molecular Formula:C₂₁H₃₇NO₃Si
Molecular Weight:379.615
Hs Code.:
Mol file:1072091-11-2.mol

C<sub>21</sub>H<sub>37</sub>NO<sub>3</sub>Si

Synonyms:C₂₁H₃₇NO₃Si

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Chemical Property of C₂₁H₃₇NO₃Si Edit

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Technology Process of C₂₁H₃₇NO₃Si

There total 6 articles about C₂₁H₃₇NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1072091-06-5
ethyl (2E,4S,5R)-6-{[tert-butyl(dimethyl)silyl]oxy}-4-[(4-methoxyphenyl)amino]-3,5-dimethylhex-2-enoate

: 1072091-11-2
C₂₁H₃₇NO₃Si

Guidance literature:: ethyl (2E,4S,5R)-6-{[tert-butyl(dimethyl)silyl]oxy}-4-[(4-methoxyphenyl)amino]-3,5-dimethylhex-2-enoate; With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 ℃; for 0.5h;

With sodium potassium tartrate; water; In hexane; dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 124156-21-4
ethyl (4-methoxyphenylimino)acetate

: 1072091-11-2
C₂₁H₃₇NO₃Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: (3R,5R)-5-methyl-3-pyrrolidinecarboxylic acid / dimethyl sulfoxide / 1 h / 20 °C

2.1: sodium tetrahydroborate / methanol; dimethyl sulfoxide / 0.5 h / 0 °C

3.1: 1H-imidazole / N,N-dimethyl-formamide / 10.5 h / 20 °C

4.1: lithium hexamethyldisilazane / tetrahydrofuran / 1.5 h / -10 °C

5.1: tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

6.1: toluene / 36 h / Heating / reflux

6.2: 1 h / 0 °C

7.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 °C

7.2: 1 h / 0 °C

With 1H-imidazole; sodium tetrahydroborate; diisobutylaluminium hydride; lithium hexamethyldisilazane; (3R,5R)-5-methyl-3-pyrrolidinecarboxylic acid; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 409095-87-0
ethyl (2S,3R)-3-formyl-2-(4-methoxyphenylamino)butanoate

: 1072091-11-2
C₂₁H₃₇NO₃Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tetrahydroborate / methanol; dimethyl sulfoxide / 0.5 h / 0 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 10.5 h / 20 °C

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 1.5 h / -10 °C

4.1: tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

5.1: toluene / 36 h / Heating / reflux

5.2: 1 h / 0 °C

6.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 °C

6.2: 1 h / 0 °C

With 1H-imidazole; sodium tetrahydroborate; diisobutylaluminium hydride; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;