1-[(4-nitrophenyl)sulphanyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine

Base Information

• Chemical Name: 1-[(4-nitrophenyl)sulphanyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine
• CAS No.: 930285-83-9
• Molecular Formula: C₁₁H₁₂N₂O₄S
• Molecular Weight: 268.293

Synonyms:1-[(4-nitrophenyl)sulphanyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine

Chemical Property of 1-[(4-nitrophenyl)sulphanyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine

Chemical Property:

Purity/Quality:

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Technology Process of 1-[(4-nitrophenyl)sulphanyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine

There total 2 articles about 1-[(4-nitrophenyl)sulphanyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

4-nitrobenzenesulfenyl chloride (937-32-6) + 1a,2,6,6a-tetrahydro-1H,4H-<1,3>-dioxepino<5,6-b>azirine (151021-81-7) → 1-[(4-nitrophenyl)sulphanyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine (930285-83-9) + 1-[(4-nitrophenyl)sulphinyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine + 1-<(4-nitrophenyl)sulfonyl>-1a,2,6,6a-tetrahydro-1H,4H-<1,3>dioxepino<5,6-b>azirine (169614-08-8)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 0.25h;

Reference yield: 26.0%

4-nitrobenzenesulfenyl chloride (937-32-6) + 1a,2,6,6a-tetrahydro-1H,4H-<1,3>-dioxepino<5,6-b>azirine (151021-81-7) → 1-[(4-nitrophenyl)sulphanyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine (930285-83-9) + 1-[(4-nitrophenyl)sulphinyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine

Guidance literature:

With pyridine; air; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield: 67.0%

1-[(4-nitrophenyl)sulphanyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine (930285-83-9) → 1-[(4-nitrophenyl)sulphinyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine + 1-<(4-nitrophenyl)sulfonyl>-1a,2,6,6a-tetrahydro-1H,4H-<1,3>dioxepino<5,6-b>azirine (169614-08-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃;

upstream raw materials:

4-nitrobenzenesulfenyl chloride

1a,2,6,6a-tetrahydro-1H,4H-<1,3>-dioxepino<5,6-b>azirine

Downstream raw materials:

1-<(4-nitrophenyl)sulfonyl>-1a,2,6,6a-tetrahydro-1H,4H-<1,3>dioxepino<5,6-b>azirine

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