PtCl₂(pyridine-2-CHN₆H₄OMe-p)

Base Information

• Chemical Name: PtCl₂(pyridine-2-CHN₆H₄OMe-p)
• CAS No.: 113872-74-5
• Molecular Formula: C₁₃H₁₂Cl₂N₂OPt
• Molecular Weight: 478.237
• Mol file: 113872-74-5.mol

Synonyms:PtCl₂(pyridine-2-CHN₆H₄OMe-p)

Chemical Property of PtCl₂(pyridine-2-CHN₆H₄OMe-p)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of PtCl₂(pyridine-2-CHN₆H₄OMe-p)

There total 3 articles about PtCl₂(pyridine-2-CHN₆H₄OMe-p) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

potassium tetrachloroplatinate(II) (10025-99-7) + N-(pyrid-2-ylmethylene)-p-methoxyphenylamine (26930-67-6) → PtCl2(pyridine-2-CHN6H4OMe-p) (113872-74-5)

Guidance literature:

In hydrogenchloride; water; organic ligand added to a soln. of K2PtCl4 in water acidified with aq. HCl; stirred for 1 h at 100°C; cooled to room temp.; filtered off; washed with water, cold CH3OH, Et2O;dried in vacuo; elem. anal.;

DOI:10.1002/zaac.200600032

Reference yield: 58.5%

N-(pyrid-2-ylmethylene)-p-methoxyphenylamine (26930-67-6) + Zeise's salt (16405-35-9) → PtCl2(pyridine-2-CHN6H4OMe-p) (113872-74-5)

Guidance literature:

In methanol; dichloromethane; room temp., stirring for 10 min, pptn.,; evapn., extn. with boiling CH2Cl2, pptn. by diluting concd. soln. with Et2O, elem. anal.;

DOI:10.1016/S0020-1693(00)83917-1

Reference yield:

N-(pyrid-2-ylmethylene)-p-methoxyphenylamine (26930-67-6) + PtCl2(C6H4OMe-p)NCHCHN(C6H4OMe-p) (113872-72-3) → PtCl2(pyridine-2-CHN6H4OMe-p) (113872-74-5)

Guidance literature:

In dimethylsulfoxide-d6; room temp., equimolar amts., (1)H NMR control, fast reaction;

DOI:10.1016/S0020-1693(00)83917-1

upstream raw materials:

N-(pyrid-2-ylmethylene)-p-methoxyphenylamine

PtCl₂(C₆H₄OMe-p)NCHCHN(C₆H₄OMe-p)

Zeise's salt

potassium tetrachloroplatinate(II)

Downstream raw materials:

platinum

PtCl₂(C₆H₄OMe-p)NCHCHN(C₆H₄OMe-p)

dichloro(2,2'-bipyridine)platinum(II)