(-)-(1'S,1''S)-<(2-Oxocyclohexyl)phenylmethyl>propandisaeure-diethylester

Base Information

Chemical Name:(-)-(1'S,1''S)-<(2-Oxocyclohexyl)phenylmethyl>propandisaeure-diethylester
CAS No.:86661-22-5
Molecular Formula:C₂₀H₂₆O₅
Molecular Weight:346.423
Hs Code.:

Synonyms:(-)-(1'S,1''S)-<(2-Oxocyclohexyl)phenylmethyl>propandisaeure-diethylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(1'S,1''S)-<(2-Oxocyclohexyl)phenylmethyl>propandisaeure-diethylester

Chemical Property:

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Technology Process of (-)-(1'S,1''S)-<(2-Oxocyclohexyl)phenylmethyl>propandisaeure-diethylester

There total 12 articles about (-)-(1'S,1''S)-<(2-Oxocyclohexyl)phenylmethyl>propandisaeure-diethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 5292-53-5
diethyl benzalmalonate

: 86661-22-5,133616-99-6
(+)-(1'R,1''R)-<(2-Oxocyclohexyl)phenylmethyl>propandisaeure-diethylester

: 86661-22-5
(-)-(1'S,1''S)-<(2-Oxocyclohexyl)phenylmethyl>propandisaeure-diethylester

Guidance literature:: (S)-2-(1-pyrrolidinylmethyl)pyrrolidine; In tetrahydrofuran; at 25 ℃; for 96h;
DOI:10.1016/S0040-4039(01)00793-6

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 5292-53-5
diethyl benzalmalonate

: 86661-22-5,133616-99-6
(+)-(1'R,1''R)-<(2-Oxocyclohexyl)phenylmethyl>propandisaeure-diethylester

: 86661-22-5
(-)-(1'S,1''S)-<(2-Oxocyclohexyl)phenylmethyl>propandisaeure-diethylester

Guidance literature:: (S)-2-(1-pyrrolidinylmethyl)pyrrolidine; In tetrahydrofuran; at 25 ℃; for 96h;
DOI:10.1016/S0040-4039(01)00793-6

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 5292-53-5
diethyl benzalmalonate

: 86661-22-5,133616-99-6
[(2-oxo-cyclohexyl)-phenyl-methyl]-malonic acid diethyl ester

: 86661-22-5,133616-99-6
(+)-(1'R,1''R)-<(2-Oxocyclohexyl)phenylmethyl>propandisaeure-diethylester

: 86661-22-5
(-)-(1'S,1''S)-<(2-Oxocyclohexyl)phenylmethyl>propandisaeure-diethylester

Guidance literature:: With N-(((2S,4R)-4-(tert-butyldimethylsilyloxy)pyrrolidin-2-yl)methyl)-1,1,1-trifluoromethanesulfonamide; at 20 ℃; for 336h; Title compound not separated from byproducts.;
DOI:10.1021/jo070070p