4-(methylsulfanyl)-2-{3-[4-(methylsulfanyl)-2',6-bipyridin-2-yl]phenyl}-2',6-bipyridine

Base Information

Chemical Name:4-(methylsulfanyl)-2-{3-[4-(methylsulfanyl)-2',6-bipyridin-2-yl]phenyl}-2',6-bipyridine
CAS No.:138336-93-3
Molecular Formula:C₂₈H₂₂N₄S₂
Molecular Weight:478.641
Hs Code.:
Mol file:138336-93-3.mol

Synonyms:1,3-bis-(4-methylthio-2,2'-bipyridin-6-yl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(methylsulfanyl)-2-{3-[4-(methylsulfanyl)-2',6-bipyridin-2-yl]phenyl}-2',6-bipyridine

Chemical Property:

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Technology Process of 4-(methylsulfanyl)-2-{3-[4-(methylsulfanyl)-2',6-bipyridin-2-yl]phenyl}-2',6-bipyridine

There total 3 articles about 4-(methylsulfanyl)-2-{3-[4-(methylsulfanyl)-2',6-bipyridin-2-yl]phenyl}-2',6-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6781-42-6
1,3-diacetylbenzene

: 78570-34-0
3,3-bis(methylsulfanyl)-1-pyridin-2-ylprop-2-en-1-one

: 138336-93-3
1,3-bis-(4-methylthio-2,2'-bipyridin-6-yl)benzene

Guidance literature:: With ammonium acetate; potassium tert-butylate; acetic acid; Yield given. Multistep reaction; 1.) THF, room temp., 4 h 2.) reflux, 3 h;
DOI:10.1039/DT9930001883

Reference yield:

: 6781-42-6
1,3-diacetylbenzene

: 138336-93-3
1,3-bis-(4-methylthio-2,2'-bipyridin-6-yl)benzene

Guidance literature:: Multi-step reaction with 2 steps

2: 1) KOtBu, 2) NH₄OAc / 2) AcOH, heating

With potassium tert-butylate; ammonium acetate;