2,2'-Bipyridine, 6,6''-(1,3-phenylene)bis-

Base Information

Chemical Name:2,2'-Bipyridine, 6,6''-(1,3-phenylene)bis-
CAS No.:138336-94-4
Molecular Formula:C26H18N4
Molecular Weight:386.44800
Hs Code.:
Mol file:138336-94-4.mol

Synonyms:2,2'-Bipyridine,6,6''-(1,3-phenylene)bis;1,3-bis(2,2'-bipyridin-6-yl)benzene;

Suppliers and Price of 2,2'-Bipyridine, 6,6''-(1,3-phenylene)bis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2,2'-Bipyridine, 6,6''-(1,3-phenylene)bis-

Chemical Property:

PSA：51.56000
LogP:5.93460

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,2'-Bipyridine, 6,6''-(1,3-phenylene)bis-

There total 6 articles about 2,2'-Bipyridine, 6,6''-(1,3-phenylene)bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 138336-93-3
1,3-bis-(4-methylthio-2,2'-bipyridin-6-yl)benzene

: 138336-94-4
1,3-bis-(2,2'-bipyridin-6-yl)benzene

Guidance literature:: With sodium hydroxide; sodium tetrahydroborate; nickel dichloride; In ethanol; for 24h; Heating;
DOI:10.1039/DT9930001883

Reference yield: 30.0%

: 26482-00-8
1-(2-oxo-2-(2-pyridyl)ethyl)pyridinium iodide

: 1,3-bis[1-oxo-3-(dimethylamino)propyl]benzene dihydrochloride

: 138336-94-4
1,3-bis-(2,2'-bipyridin-6-yl)benzene

Guidance literature:: With ammonium acetate; acetic acid; for 4h; Heating;
DOI:10.1039/DT9930001883

Reference yield:

: 6781-42-6
1,3-diacetylbenzene

: 138336-94-4
1,3-bis-(2,2'-bipyridin-6-yl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium t-butoxide 2.) ammonium acetate, acetic acid / 1.) THF, room temp., 4 h 2.) reflux, 3 h

2: 60 percent / NiCl₂*6H₂O, NaBH₄, 40percent aq. sodium hydroxide / ethanol / 24 h / Heating

With ammonium acetate; sodium hydroxide; sodium tetrahydroborate; potassium tert-butylate; acetic acid; nickel dichloride; In ethanol;
DOI:10.1039/DT9930001883