t-butyl [(2E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)prop-2-en-1-yl]carbamate

Base Information

Chemical Name:t-butyl [(2E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)prop-2-en-1-yl]carbamate
CAS No.:1432514-66-3
Molecular Formula:C₁₅H₂₁NO₃
Molecular Weight:263.337
Hs Code.:

Synonyms:t-butyl [(2E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)prop-2-en-1-yl]carbamate

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Chemical Property of t-butyl [(2E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)prop-2-en-1-yl]carbamate

Chemical Property:

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Technology Process of t-butyl [(2E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)prop-2-en-1-yl]carbamate

There total 1 articles about t-butyl [(2E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)prop-2-en-1-yl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5159-41-1
2-iodobenzyl alcohol

: 468060-28-8
(E)-tert-butyl (3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)prop-2-en-1-yl)carbamate

: 1432514-66-3
t-butyl [(2E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)prop-2-en-1-yl]carbamate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; In tetrahydrofuran; water; at 120 ℃; for 0.166667h; Concentration; Time; Solvent; Microwave irradiation;

Reference yield:

: 1432514-66-3
t-butyl [(2E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)prop-2-en-1-yl]carbamate

: 1432515-05-3
tert-butyl (3-(2-(hydroxymethyl)phenyl)propyl)carbamate

Guidance literature:: With palladium on activated charcoal; hydrogen; In methanol; at 18 - 25 ℃; for 2h; Inert atmosphere;

Reference yield:

: 1432514-66-3
t-butyl [(2E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)prop-2-en-1-yl]carbamate

: 1432513-74-0
(R)-3-(1-(2-(3-aminopropyl)phenyl)ethyl)-5-fluoro-2-oxo-N-(1,2,4-thiadiazol-5-yl)-2,3-dihydrobenzo[d]oxazole-6-sulfonamide trifluoroacetate

Guidance literature:: Multi-step reaction with 6 steps

1: palladium on activated charcoal; hydrogen / methanol / 2 h / 18 - 25 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 1.67 h / 0 °C

3: diethyl ether / 0 - 25 °C

4: ChiralTech IC column / Resolution of racemate

5: diethylazodicarboxylate; triphenylphosphine / tetrahydrofuran / 18 h / 0 - 25 °C

6: dichloromethane / 0.5 h / 18 - 25 °C

With palladium on activated charcoal; hydrogen; Dess-Martin periodane; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;