allyl 4-oxocyclohexanecarboxylate

Base Information

• Chemical Name: allyl 4-oxocyclohexanecarboxylate
• CAS No.: 945843-03-8
• Molecular Formula: C₁₀H₁₄O₃
• Molecular Weight: 182.219
• Mol file: 945843-03-8.mol

Synonyms:allyl 4-oxocyclohexanecarboxylate

Chemical Property of allyl 4-oxocyclohexanecarboxylate

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of allyl 4-oxocyclohexanecarboxylate

There total 1 articles about allyl 4-oxocyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-oxocyclohexanecarboxylic acid (874-61-3) + allyl bromide (106-95-6) → allyl 4-oxocyclohexanecarboxylate (945843-03-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h;

DOI:10.1002/chem.200700108

Reference yield:

allyl 4-oxocyclohexanecarboxylate (945843-03-8) + chloro-trimethyl-silane (75-77-4) → C13H22O3Si

Guidance literature:

With sodium hydride; In diethyl ether; at 0 ℃; for 1h;

DOI:10.1002/chem.200700108

Reference yield:

allyl 4-oxocyclohexanecarboxylate (945843-03-8) → allyl 15-[(4-methoxybenzyl)oxy]-7,11,18,21-tetraoxatrispiro[5.2.2.5.2.2]henicosane-3-carboxylate (945843-15-2)

Guidance literature:

Multi-step reaction with 2 steps

1: NaH / diethyl ether / 1 h / 0 °C

2: 3.33 g / trimethylsilyl triflate / diethyl ether / 20 °C

With trimethylsilyl trifluoromethanesulfonate; sodium hydride; In diethyl ether;

DOI:10.1002/chem.200700108

upstream raw materials:

4-oxocyclohexanecarboxylic acid

allyl bromide

Downstream raw materials:

allyl 15-[(4-methoxybenzyl)oxy]-7,11,18,21-tetraoxatrispiro[5.2.2.5.2.2]henicosane-3-carboxylate