3',5'-O-bis(tert-butyldimethylsilyl)-N-benzoyl-5-([D₃]methyl)-2'-deoxycytidine

Base Information

Chemical Name:3',5'-O-bis(tert-butyldimethylsilyl)-N-benzoyl-5-([D₃]methyl)-2'-deoxycytidine
CAS No.:1280736-12-0
Molecular Formula:C₂₉H₄₇N₃O₅Si₂
Molecular Weight:576.856
Hs Code.:

3',5'-O-bis(tert-butyldimethylsilyl)-N-benzoyl-5-([D<sub>3</sub>]methyl)-2'-deoxycytidine

Synonyms:3',5'-O-bis(tert-butyldimethylsilyl)-N-benzoyl-5-([D₃]methyl)-2'-deoxycytidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3',5'-O-bis(tert-butyldimethylsilyl)-N-benzoyl-5-([D₃]methyl)-2'-deoxycytidine

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Technology Process of 3',5'-O-bis(tert-butyldimethylsilyl)-N-benzoyl-5-([D₃]methyl)-2'-deoxycytidine

There total 3 articles about 3',5'-O-bis(tert-butyldimethylsilyl)-N-benzoyl-5-([D₃]methyl)-2'-deoxycytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1245724-75-7
3',5'-O-bis(tert-butyldimethylsilyl)-5-([D₃]methyl)-2'-deoxycytidine

: 98-88-4
benzoyl chloride

: 1280736-12-0
3',5'-O-bis(tert-butyldimethylsilyl)-N-benzoyl-5-([D₃]methyl)-2'-deoxycytidine

Guidance literature:: With dmap; In dichloromethane; at 20 ℃;
DOI:10.1002/chem.201001884

Reference yield:

: 1280736-11-9
4-(N-1-triazolyl)-3',5'-O-bis(tert-butyldimethylsilyl)-5-([D₃]methyl)-2'-deoxyuridine

: 1280736-12-0
3',5'-O-bis(tert-butyldimethylsilyl)-N-benzoyl-5-([D₃]methyl)-2'-deoxycytidine

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium-d₄ deuteroxide / acetonitrile / 4 h / 20 °C

2: dmap / dichloromethane / 20 °C

With dmap; ammonium-d₄ deuteroxide; In dichloromethane; acetonitrile;
DOI:10.1002/chem.201001884

Reference yield:

: 1280736-10-8
5-(trideuteromethyl)-3′,5′-(tert-butyl-dimethylsilyl)-2′-deoxyuridine

: 1280736-12-0
3',5'-O-bis(tert-butyldimethylsilyl)-N-benzoyl-5-([D₃]methyl)-2'-deoxycytidine

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; trichlorophosphate / acetonitrile / 0 °C

2: ammonium-d₄ deuteroxide / acetonitrile / 4 h / 20 °C

3: dmap / dichloromethane / 20 °C

With dmap; ammonium-d₄ deuteroxide; triethylamine; trichlorophosphate; In dichloromethane; acetonitrile;
DOI:10.1002/chem.201001884