(S)-(-)-1-[1-methyl-3-phenylpropylideneamino]-2-(methoxymethyl)pyrrolidine

Base Information

Chemical Name:(S)-(-)-1-[1-methyl-3-phenylpropylideneamino]-2-(methoxymethyl)pyrrolidine
CAS No.:175430-70-3
Molecular Formula:C₁₆H₂₄N₂O
Molecular Weight:260.379
Hs Code.:

Synonyms:(S)-(-)-1-[1-methyl-3-phenylpropylideneamino]-2-(methoxymethyl)pyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(-)-1-[1-methyl-3-phenylpropylideneamino]-2-(methoxymethyl)pyrrolidine

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Technology Process of (S)-(-)-1-[1-methyl-3-phenylpropylideneamino]-2-(methoxymethyl)pyrrolidine

There total 1 articles about (S)-(-)-1-[1-methyl-3-phenylpropylideneamino]-2-(methoxymethyl)pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2550-26-7
4-Phenyl-2-butanone

: 59983-39-0,187035-29-6
(S)-1-amino-2-(methoxymethyl)pyrrolidine

: 175430-70-3
(S)-(-)-1-[1-methyl-3-phenylpropylideneamino]-2-(methoxymethyl)pyrrolidine

Guidance literature:: In benzene; for 20h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetasy.2010.04.042

Reference yield: 80.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 175430-70-3
(S)-(-)-1-[1-methyl-3-phenylpropylideneamino]-2-(methoxymethyl)pyrrolidine

: 175430-75-8
(+)-(2S)-1-<1'-(t-Butyldimethylsilyl)-4'-phenylbut-2'-ylideneamino>-2-methoxymethylpyrrolidine

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; 1.) 0 deg C, 4 h, 2.) -78 deg C, 1 h; -78 deg C -> room temp.;

Reference yield:

: 79-22-1
methyl chloroformate

: 175430-70-3
(S)-(-)-1-[1-methyl-3-phenylpropylideneamino]-2-(methoxymethyl)pyrrolidine

: 1-[N-methoxycarbonyl-N-(1-methyl-3-phenylpropyl)amino]-2-(methoxymethyl)pyrrolidine

: 107300-18-5
(2S,2''R)-1-[N-methoxycarbonyl-N-(1-methyl-3-phenylpropyl)amino]-2-(methoxymethyl)pyrrolidine

Guidance literature:: (S)-(-)-1-[1-methyl-3-phenylpropylideneamino]-2-(methoxymethyl)pyrrolidine; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

methyl chloroformate; In tetrahydrofuran; Inert atmosphere;
DOI:10.1016/j.tetasy.2010.04.042