C₂₀H₃₁NO₃

Base Information

Chemical Name:C₂₀H₃₁NO₃
CAS No.:1630067-63-8
Molecular Formula:C₂₀H₃₁NO₃
Molecular Weight:333.471
Hs Code.:

C<sub>20</sub>H<sub>31</sub>NO<sub>3</sub>

Synonyms:C₂₀H₃₁NO₃

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Chemical Property of C₂₀H₃₁NO₃

Chemical Property:

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Technology Process of C₂₀H₃₁NO₃

There total 3 articles about C₂₀H₃₁NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1630067-62-7
(2S,3R,E)-3-[2-(benzyloxy)ethyl]-6-(methoxymethoxy)-2-(prop-1-en-2-yl)hex-4-enamide

: 1630067-63-8
C₂₀H₃₁NO₃

Guidance literature:: With aluminum (III) chloride; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at 0 ℃; for 12h; Inert atmosphere;
DOI:10.1002/ejoc.201402452

Reference yield:

: 1630067-58-1
(R,E)-6-(benzyloxy)-1-(methoxymethoxy)hex-3-en-2-ol

: 1630067-63-8
C₂₀H₃₁NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 5.17 h / 0 °C / Inert atmosphere

2.1: chloro-trimethyl-silane; lithium hexamethyldisilazane / tetrahydrofuran; diethyl ether / 2.83 h / -78 - -20 °C / Inert atmosphere

3.1: di-tert-butyl dicarbonate; pyridine / ethyl acetate / 3 h / 20 °C / Inert atmosphere

3.2: 2 h / Inert atmosphere

4.1: aluminum (III) chloride; lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 12 h / 0 °C / Inert atmosphere

With pyridine; dmap; aluminum (III) chloride; lithium aluminium tetrahydride; chloro-trimethyl-silane; di-tert-butyl dicarbonate; dicyclohexyl-carbodiimide; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1002/ejoc.201402452

Reference yield:

: 1630067-59-2
(R,E)-6-(benzyloxy)-1-(methoxymethoxy)hex-3-en-2-yl 3-methylbut-3-enoate

: 1630067-63-8
C₂₀H₃₁NO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: chloro-trimethyl-silane; lithium hexamethyldisilazane / tetrahydrofuran; diethyl ether / 2.83 h / -78 - -20 °C / Inert atmosphere

2.1: di-tert-butyl dicarbonate; pyridine / ethyl acetate / 3 h / 20 °C / Inert atmosphere

2.2: 2 h / Inert atmosphere

3.1: aluminum (III) chloride; lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 12 h / 0 °C / Inert atmosphere

With pyridine; aluminum (III) chloride; lithium aluminium tetrahydride; chloro-trimethyl-silane; di-tert-butyl dicarbonate; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; ethyl acetate;
DOI:10.1002/ejoc.201402452