(R)-4-chloro-3-(1-(2,4-dichlorophenyl)ethylamino)phenyl trifluoromethanesulfonate

Base Information

Chemical Name:(R)-4-chloro-3-(1-(2,4-dichlorophenyl)ethylamino)phenyl trifluoromethanesulfonate
CAS No.:1441792-25-1
Molecular Formula:C₁₅H₁₁Cl₃F₃NO₃S
Molecular Weight:448.677
Hs Code.:

Synonyms:(R)-4-chloro-3-(1-(2,4-dichlorophenyl)ethylamino)phenyl trifluoromethanesulfonate

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Chemical Property of (R)-4-chloro-3-(1-(2,4-dichlorophenyl)ethylamino)phenyl trifluoromethanesulfonate

Chemical Property:

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Technology Process of (R)-4-chloro-3-(1-(2,4-dichlorophenyl)ethylamino)phenyl trifluoromethanesulfonate

There total 6 articles about (R)-4-chloro-3-(1-(2,4-dichlorophenyl)ethylamino)phenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89981-75-9
1-(2',4'-dichlorophenyl)ethylamine

: 1441792-25-1
(R)-4-chloro-3-(1-(2,4-dichlorophenyl)ethylamino)phenyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: (S)-Mandelic acid / isopropyl alcohol; ethanol / 26 h / 30 - 60 °C

1.2: 1 h / 20 °C

2.1: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 3 h / 110 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4.5 h / 0 - 20 °C

4.1: triethylamine / dichloromethane / 2 h / 0 °C

With (S)-Mandelic acid; tetrabutyl ammonium fluoride; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; sodium t-butanolate; In tetrahydrofuran; ethanol; dichloromethane; isopropyl alcohol; toluene;

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 1441792-20-6
(R)-4-chloro-3-(1-(2,4-dichlorophenyl)ethylamino)phenol

: 1441792-25-1
(R)-4-chloro-3-(1-(2,4-dichlorophenyl)ethylamino)phenyl trifluoromethanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 2h;

Reference yield:

: 151692-21-6
(3-bromo-4-chloro-phenoxy)-tert-butyl-dimethyl-silane

: 1441792-25-1
(R)-4-chloro-3-(1-(2,4-dichlorophenyl)ethylamino)phenyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 3 h / 110 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 4.5 h / 0 - 20 °C

3: triethylamine / dichloromethane / 2 h / 0 °C

With tetrabutyl ammonium fluoride; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; sodium t-butanolate; In tetrahydrofuran; dichloromethane; toluene;