(C₅H₅)(CO)(P(C₂H₅)3)FeC(OCH₃)C₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=(C₅H₅)(CO)(P(C₂H₅)3)FeC(OCH₃)C₆H₅O₃SCF₃

Base Information

• Chemical Name: (C₅H₅)(CO)(P(C₂H₅)3)FeC(OCH₃)C₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=(C₅H₅)(CO)(P(C₂H₅)3)FeC(OCH₃)C₆H₅O₃SCF₃
• CAS No.: 117094-57-2
• Molecular Formula: CF₃O₃S*C₂₀H₂₈FeO₂P
• Molecular Weight: 536.332

Synonyms:(C₅H₅)(CO)(P(C₂H₅)3)FeC(OCH₃)C₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=(C₅H₅)(CO)(P(C₂H₅)3)FeC(OCH₃)C₆H₅O₃SCF₃

Chemical Property of (C₅H₅)(CO)(P(C₂H₅)3)FeC(OCH₃)C₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=(C₅H₅)(CO)(P(C₂H₅)3)FeC(OCH₃)C₆H₅O₃SCF₃

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Technology Process of (C₅H₅)(CO)(P(C₂H₅)3)FeC(OCH₃)C₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=(C₅H₅)(CO)(P(C₂H₅)3)FeC(OCH₃)C₆H₅O₃SCF₃

There total 1 articles about (C₅H₅)(CO)(P(C₂H₅)3)FeC(OCH₃)C₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=(C₅H₅)(CO)(P(C₂H₅)3)FeC(OCH₃)C₆H₅O₃SCF₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(C5H5)(CO)(P(C2H5)3)FeCOC6H5 (117094-53-8) + methyl trifluoromethanesulfonate (333-27-7) → (C5H5)(CO)(P(C2H5)3)FeC(OCH3)C6H5(1+)*CF3SO3(1-)=(C5H5)(CO)(P(C2H5)3)FeC(OCH3)C6H5O3SCF3 (117094-57-2)

Guidance literature:

In dichloromethane; 2 equiv. of MeOTf are added to a soln. of Fe complex and stirred at room temp. overnight.; filtn. through Celite, removal of solvent in vacuo, washing with Et2O;

DOI:10.1021/ja00184a025

Reference yield: 93.0%

sodium tetrahydroborate (16940-66-2) + (C5H5)(CO)(P(C2H5)3)FeC(OCH3)C6H5(1+)*CF3SO3(1-)=(C5H5)(CO)(P(C2H5)3)FeC(OCH3)C6H5O3SCF3 (117094-57-2) + sodium methylate (124-41-4) → (C5H5)(CO)(P(C2H5)3)FeCH(OCH3)C6H5 (117178-89-9)

Guidance literature:

In methanol; dichloromethane; A soln. of Fe complex in CH2Cl2 is added dropwise to a rapidly stirring CH3OH/CH3ONa/NaBH4 soln. at 0°C.; Soln. is stirred with CH2Cl2/aq. NaHCO3, and the CH2Cl2 layer is filtered through Celite/anhydrous K2CO3. Solvent is removed in vacuo.;

DOI:10.1021/ja00184a025

upstream raw materials:

(C₅H₅)(CO)(P(C₂H₅)3)FeCOC₆H₅

methyl trifluoromethanesulfonate

Downstream raw materials:

(C₅H₅)(CO)(P(C₂H₅)3)FeCH(OCH₃)C₆H₅

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