C₃₃H₃₉ClN₂O₅

Base Information

Chemical Name:C₃₃H₃₉ClN₂O₅
CAS No.:1338706-96-9
Molecular Formula:C₃₃H₃₉ClN₂O₅
Molecular Weight:579.136
Hs Code.:

C<sub>33</sub>H<sub>39</sub>ClN<sub>2</sub>O<sub>5</sub>

Synonyms:C₃₃H₃₉ClN₂O₅

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Chemical Property of C₃₃H₃₉ClN₂O₅

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Technology Process of C₃₃H₃₉ClN₂O₅

There total 6 articles about C₃₃H₃₉ClN₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 2-chloro-3,4-bis[(4-methoxyphenyl)methoxy]benzoic acid

: 13323-42-7
3-methyl-3,9-diaza-spiro[5.5]undecane dihydrochloride

: 1338706-96-9
C₃₃H₃₉ClN₂O₅

Guidance literature:: 2-chloro-3,4-bis[(4-methoxyphenyl)methoxy]benzoic acid; With methanesulfonyl chloride; triethylamine; In N,N-dimethyl acetamide; at -15 ℃; for 1h;

3-methyl-3,9-diaza-spiro[5.5]undecane dihydrochloride; With triethylamine; In N,N-dimethyl acetamide; at -15 ℃; for 2h;

Reference yield:

: 13323-40-5
3-benzyl-9-methyl-3,9-diaza-spiro[5.5]undecane

: 1338706-96-9
C₃₃H₃₉ClN₂O₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid; 5%-palladium/activated carbon; hydrogen / 48 h / 20 °C / 3800.26 Torr

2.1: methanesulfonyl chloride; triethylamine / N,N-dimethyl acetamide / 1 h / -15 °C

2.2: 2 h / -15 °C

With 5%-palladium/activated carbon; hydrogen; acetic acid; methanesulfonyl chloride; triethylamine; In N,N-dimethyl acetamide;

Reference yield:

: 3612-20-2
1-phenylmethyl-4-piperidone

: 1338706-96-9
C₃₃H₃₉ClN₂O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: ammonia / methanol / 4.8 h / 0 - 4 °C

2.1: sulfuric acid / water / 16 h / Reflux

2.2: 20 °C / pH 8

3.1: lithium aluminium tetrahydride / diethyl ether / 16 h / Reflux

4.1: formic acid / water; tetrahydrofuran / 3 h / 100 °C

4.2: 20 °C / pH 10

5.1: acetic acid; 5%-palladium/activated carbon; hydrogen / 48 h / 20 °C / 3800.26 Torr

6.1: methanesulfonyl chloride; triethylamine / N,N-dimethyl acetamide / 1 h / -15 °C

6.2: 2 h / -15 °C

With lithium aluminium tetrahydride; formic acid; sulfuric acid; 5%-palladium/activated carbon; ammonia; hydrogen; acetic acid; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl acetamide; water;