3,5-di-O-benzyl-1,2-O-isopropylidene-5-C-phenyl-α-D-gluco-pentafuranose

Base Information

Chemical Name:3,5-di-O-benzyl-1,2-O-isopropylidene-5-C-phenyl-α-D-gluco-pentafuranose
CAS No.:144402-16-4
Molecular Formula:C₂₈H₃₀O₅
Molecular Weight:446.543
Hs Code.:

Synonyms:3,5-di-O-benzyl-1,2-O-isopropylidene-5-C-phenyl-α-D-gluco-pentafuranose

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Chemical Property of 3,5-di-O-benzyl-1,2-O-isopropylidene-5-C-phenyl-α-D-gluco-pentafuranose

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Technology Process of 3,5-di-O-benzyl-1,2-O-isopropylidene-5-C-phenyl-α-D-gluco-pentafuranose

There total 11 articles about 3,5-di-O-benzyl-1,2-O-isopropylidene-5-C-phenyl-α-D-gluco-pentafuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 100-39-0
benzyl bromide

: 18439-43-5,18439-42-4
3-O-benzyl-1,2-O-isopropylidene-5-C-phenyl-α-D-gluco-pentafuranose

: 144402-16-4
3,5-di-O-benzyl-1,2-O-isopropylidene-5-C-phenyl-α-D-gluco-pentafuranose

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2006.09.005

Reference yield:

: 20715-20-2
3-O-benzyl-1,2-O-isopropylidene-5-C-phenyl-α-D-xylo-pent-5-ulo-furanose

: 144402-16-4
3,5-di-O-benzyl-1,2-O-isopropylidene-5-C-phenyl-α-D-gluco-pentafuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / NaBH₄ / methanol / 4 h / 0 - 20 °C

2: 98 percent / NaH; TBAI / tetrahydrofuran / 2 h / 20 °C

With sodium tetrahydroborate; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; methanol;
DOI:10.1016/j.tet.2006.09.005

Reference yield:

: 23558-05-6
3-O-benzyl-1,2-O-isopropylidene-1,5-D-xylo-dialdofuranose

: 144402-16-4
3,5-di-O-benzyl-1,2-O-isopropylidene-5-C-phenyl-α-D-gluco-pentafuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 7 percent / tetrahydrofuran / 12 h / 20 °C

2: 98 percent / NaH; TBAI / tetrahydrofuran / 2 h / 20 °C

With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran;
DOI:10.1016/j.tet.2006.09.005