(+/-)-α-methylbenzylamine-d9

Base Information

Chemical Name:(+/-)-α-methylbenzylamine-d9
CAS No.:274682-99-4
Molecular Formula:C₈H₁₁N
Molecular Weight:130.111
Hs Code.:

Synonyms:(+/-)-α-methylbenzylamine-d9

Suppliers and Price of (+/-)-α-methylbenzylamine-d9

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-α-methylbenzylamine-d9

Chemical Property:

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Technology Process of (+/-)-α-methylbenzylamine-d9

There total 6 articles about (+/-)-α-methylbenzylamine-d9 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: acetophenone-oxime-d8

: 274682-99-4
(+/-)-α-methylbenzylamine-d9

Guidance literature:: With sodium borodeuteride; titanium tetrachloride; In 1,2-dimethoxyethane; at 20 ℃; for 14h;
DOI:10.1107/S0108768199012008

Reference yield:

: 1076-43-3
benzene-d6

: 274682-99-4
(+/-)-α-methylbenzylamine-d9

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / AlCl₃ / CS₂ / 1 h

2: 85 percent / deuterium oxide; sodium hydroxide / dioxane / 24 h / 20 °C

3: 56.7 g / sodium borodeuteride / methanol / 1 h / 0 °C

4: 70.7 g / 1 h / 20 °C

5: 35.2 g / liquide ammonia / 14 h / 20 °C

With sodium hydroxide; aluminium trichloride; sodium borodeuteride; ammonia; water-d2; In 1,4-dioxane; methanol; carbon disulfide;
DOI:10.1021/ol010108z

Reference yield:

: 19547-00-3
<2H8>Acetophenone

: 274682-99-4
(+/-)-α-methylbenzylamine-d9

Guidance literature:: Multi-step reaction with 3 steps

1: 56.7 g / sodium borodeuteride / methanol / 1 h / 0 °C

2: 70.7 g / 1 h / 20 °C

3: 35.2 g / liquide ammonia / 14 h / 20 °C

With sodium borodeuteride; ammonia; In methanol;
DOI:10.1021/ol010108z