Methyl 2,2-dimethyl-3-phenyl-3-oxiranecarboximidate

Base Information

• Chemical Name: Methyl 2,2-dimethyl-3-phenyl-3-oxiranecarboximidate
• CAS No.: 152493-92-0
• Molecular Formula: C₁₂H₁₅NO₂
• Molecular Weight: 205.257
• Mol file: 152493-92-0.mol

Synonyms:Methyl 2,2-dimethyl-3-phenyl-3-oxiranecarboximidate

Chemical Property of Methyl 2,2-dimethyl-3-phenyl-3-oxiranecarboximidate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of Methyl 2,2-dimethyl-3-phenyl-3-oxiranecarboximidate

There total 4 articles about Methyl 2,2-dimethyl-3-phenyl-3-oxiranecarboximidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

methanol (67-56-1) + 2,2-Dimethyl-3-phenyl-3-oxiranecarbonitrile (5445-32-9) → Methyl 2,2-dimethyl-3-phenyl-3-oxiranecarboximidate (152493-92-0)

Guidance literature:

sodium methylate;

DOI:10.1021/jo00075a010

Reference yield: 51.0%

methanol (67-56-1) + sodium cyanide (143-33-9,25596-52-5) + phenyl isopropyl ketone (611-70-1) → 2,2-Dimethyl-3-phenyl-3-oxiranecarbonitrile (5445-32-9) + Methyl 2,2-dimethyl-3-phenyl-3-oxiranecarboximidate (152493-92-0)

Guidance literature:

sodium methylate; potassium iodide; electrochemical oxidation; a constant current of 1.0 A; 2.2 F/mol of electricity;

DOI:10.1021/jo00075a010

Reference yield: 32.0%

sodium cyanide (143-33-9,25596-52-5) + phenyl isopropyl ketone (611-70-1) → 2,2-Dimethyl-3-phenyl-3-oxiranecarbonitrile (5445-32-9) + Methyl 2,2-dimethyl-3-phenyl-3-oxiranecarboximidate (152493-92-0)

Guidance literature:

With methanol; sodium methylate; potassium iodide; electrochemical oxidation; a constant current of 1.0 A; 2.2 F/mol of electricity;

DOI:10.1021/jo00075a010

upstream raw materials:

methanol

2,2-Dimethyl-3-phenyl-3-oxiranecarbonitrile

sodium cyanide

phenyl isopropyl ketone

Downstream raw materials:

2,2-Dimethyl-3-phenyl-3-oxiranecarbamide

Methyl 2,2-dimethyl-3-phenyl-3-oxiranecarboxylate

Refernces