allylmethyl-(3-nitrobenzyl)amine

Base Information

• Chemical Name: allylmethyl-(3-nitrobenzyl)amine
• CAS No.: 937271-55-1
• Molecular Formula: C₁₁H₁₄N₂O₂
• Molecular Weight: 206.244
• Mol file: 937271-55-1.mol

Synonyms:allylmethyl-(3-nitrobenzyl)amine

Chemical Property of allylmethyl-(3-nitrobenzyl)amine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of allylmethyl-(3-nitrobenzyl)amine

There total 2 articles about allylmethyl-(3-nitrobenzyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N-methyl-N-allylamine (627-37-2) + 3-nitro-benzaldehyde (99-61-6) → allylmethyl-(3-nitrobenzyl)amine (937271-55-1)

Guidance literature:

With sodium tris(acetoxy)borohydride; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1021/jm201112g

Reference yield:

N-methyl-N-allylamine (627-37-2) + 3-Nitrobenzyl chloride (619-23-8) → allylmethyl-(3-nitrobenzyl)amine (937271-55-1)

Guidance literature:

With sodium carbonate; In chloroform; at 65 ℃;

Reference yield: 98.0%

allylmethyl-(3-nitrobenzyl)amine (937271-55-1) → 3-[(allylmethylamino)methyl]phenylamine (937271-56-2)

Guidance literature:

With methanol; tin(II) chloride hydrate; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/jm201112g

upstream raw materials:

N-methyl-N-allylamine

3-nitro-benzaldehyde

3-Nitrobenzyl chloride

Downstream raw materials:

3-[(allylmethylamino)methyl]phenylamine

C₂₅H₂₈N₄O

but-3-enoic acid [3-(2-{3-[(allylmethylamino)methyl]phenylamino}pyrimidin-4-yl)phenyl]amide

N-allyl-3-(2-{3-[(allylmethylamino)methyl]phenylamino}pyrimidin-4-yl)benzamide