C₅₂H₅₄N₈O₈Si

Base Information

Chemical Name:C₅₂H₅₄N₈O₈Si
CAS No.:1222078-42-3
Molecular Formula:C₅₂H₅₄N₈O₈Si
Molecular Weight:947.135
Hs Code.:

C<sub>52</sub>H<sub>54</sub>N<sub>8</sub>O<sub>8</sub>Si

Synonyms:C₅₂H₅₄N₈O₈Si

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Chemical Property of C₅₂H₅₄N₈O₈Si

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Technology Process of C₅₂H₅₄N₈O₈Si

There total 7 articles about C₅₂H₅₄N₈O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.8%

: 129681-71-6,81265-93-2
5'-O-dimethoxytrityl-2'-O-tert-butyldimethylsilyl-N₆-benzoyl adenosine

: 289712-58-9
2-(azidomethyl)benzoyl chloride

: 1222078-42-3
C₅₂H₅₄N₈O₈Si

Guidance literature:: 5'-O-dimethoxytrityl-2'-O-tert-butyldimethylsilyl-N₆-benzoyl adenosine; 2-(azidomethyl)benzoyl chloride; With 1-methyl-1H-imidazole; In dichloromethane; for 40h; Cooling with ice;

With sodium hydrogencarbonate; In dichloromethane;

Reference yield:

: 2417-73-4
methyl 2-bromomethylbenzoate

: 1222078-42-3
C₅₂H₅₄N₈O₈Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium azide / ethanol / 20 °C

2.1: sodium hydroxide; water / methanol / 0.5 h / 20 °C

2.2: pH 1

3.1: thionyl chloride / chloroform / 5 h / Reflux

4.1: 1-methyl-1H-imidazole / dichloromethane / 40 h / Cooling with ice

With 1-methyl-1H-imidazole; thionyl chloride; sodium azide; water; sodium hydroxide; In methanol; ethanol; dichloromethane; chloroform;

Reference yield:

: 89-71-4
2-Methyl-benzoic acid methyl ester

: 1222078-42-3
C₅₂H₅₄N₈O₈Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 1.5 h / Reflux

2.1: sodium azide / ethanol / 20 °C

3.1: sodium hydroxide; water / methanol / 0.5 h / 20 °C

3.2: pH 1

4.1: thionyl chloride / chloroform / 5 h / Reflux

5.1: 1-methyl-1H-imidazole / dichloromethane / 40 h / Cooling with ice

With 1-methyl-1H-imidazole; N-Bromosuccinimide; thionyl chloride; sodium azide; water; sodium hydroxide; dibenzoyl peroxide; In methanol; tetrachloromethane; ethanol; dichloromethane; chloroform;