2-(benzyloxy)-5-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamide

Base Information

Chemical Name:2-(benzyloxy)-5-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamide
CAS No.:1445854-25-0
Molecular Formula:C₃₂H₄₁NO₄
Molecular Weight:503.682
Hs Code.:

Synonyms:2-(benzyloxy)-5-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamide

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Chemical Property of 2-(benzyloxy)-5-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamide

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Technology Process of 2-(benzyloxy)-5-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamide

There total 8 articles about 2-(benzyloxy)-5-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1445854-24-9
2-(benzyloxy)-5-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzoic acid

: 1445854-25-0
2-(benzyloxy)-5-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamide

Guidance literature:: 2-(benzyloxy)-5-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzoic acid; With oxalyl dichloride; Inert atmosphere;

With ammonium hydroxide; Inert atmosphere;

Reference yield:

: C₃₂H₃₉ClO₄

: 1445854-25-0
2-(benzyloxy)-5-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamide

Guidance literature:: With ammonium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2015.05.011

Reference yield:

: 176240-84-9
methyl 4-(benzyloxy)-3-bromobenzoate

: 1445854-25-0
2-(benzyloxy)-5-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamide

Guidance literature:: Multi-step reaction with 7 steps

1.1: Inert atmosphere

2.1: boron trifluoride diethyl etherate / Inert atmosphere

3.1: triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane / Inert atmosphere

4.1: potassium carbonate / Inert atmosphere

5.1: sodium tetrahydroborate / Inert atmosphere

6.1: lithium hydroxide / Inert atmosphere

7.1: oxalyl dichloride / Inert atmosphere

7.2: Inert atmosphere

With sodium tetrahydroborate; oxalyl dichloride; boron trifluoride diethyl etherate; 1,3-bis-(diphenylphosphino)propane; palladium diacetate; potassium carbonate; triethylamine; lithium hydroxide;