Technology Process of N-Fmoc-5-aminolevulinic acid
There total 4 articles about N-Fmoc-5-aminolevulinic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen bromide; acetic acid;
at 100 ℃;
for 1h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / dichloromethane / 0.5 h / 0 °C
2: sodium dihydrogenphosphate; chlorine dioxyde / water; butan-1-ol / 3 h / 0 °C
3: acetic acid; hydrogen bromide / 1 h / 100 °C / Inert atmosphere
With
sodium dihydrogenphosphate; chlorine dioxyde; hydrogen bromide; potassium carbonate; acetic acid;
In
dichloromethane; water; butan-1-ol;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium dihydrogenphosphate; chlorine dioxyde / water; butan-1-ol / 3 h / 0 °C
2: acetic acid; hydrogen bromide / 1 h / 100 °C / Inert atmosphere
With
sodium dihydrogenphosphate; chlorine dioxyde; hydrogen bromide; acetic acid;
In
water; butan-1-ol;