1-(Methoxymethoxy)methyl cyclohexyl ketone

Base Information

Chemical Name:1-(Methoxymethoxy)methyl cyclohexyl ketone
CAS No.:170451-00-0
Molecular Formula:C₁₀H₁₈O₃
Molecular Weight:186.251
Hs Code.:

Synonyms:1-(Methoxymethoxy)methyl cyclohexyl ketone

Suppliers and Price of 1-(Methoxymethoxy)methyl cyclohexyl ketone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(Methoxymethoxy)methyl cyclohexyl ketone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(Methoxymethoxy)methyl cyclohexyl ketone

There total 3 articles about 1-(Methoxymethoxy)methyl cyclohexyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 107-30-2
chloromethyl methyl ether

: 6004-53-1
1-cyclohexyl-2-hydroxyethanone

: 170451-00-0
1-(Methoxymethoxy)methyl cyclohexyl ketone

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; 1.) 0 deg C, 1 h; 2.) r.t., overnight;
DOI:10.1021/jo00121a029

Reference yield:

: 119612-85-0
{[1-cyclohexylethenyl]oxy}trimethylsilane

: 170451-00-0
1-(Methoxymethoxy)methyl cyclohexyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 85percent m-CPBA, 2.) TBAF / 1.) CH₂Cl₂, 0 deg C, 30 min; r.t., 2 h, 2.) r.t., 45 min

2: 90 percent / i-Pr₂NEt / CH₂Cl₂ / 1.) 0 deg C, 1 h; 2.) r.t., overnight

With tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jo00121a029

Reference yield:

: 823-76-7
Cyclohexyl methyl ketone

: 170451-00-0
1-(Methoxymethoxy)methyl cyclohexyl ketone

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / LDA / tetrahydrofuran / 1.) -25 deg C, 10 min, 2.) r.t., 2.5 h

2: 1.) 85percent m-CPBA, 2.) TBAF / 1.) CH₂Cl₂, 0 deg C, 30 min; r.t., 2 h, 2.) r.t., 45 min

3: 90 percent / i-Pr₂NEt / CH₂Cl₂ / 1.) 0 deg C, 1 h; 2.) r.t., overnight

With tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00121a029