2-[2-Ethoxycarbonyl-1-phenyl-eth-(E)-ylideneamino]-benzoic acid methyl ester

Base Information

Chemical Name:2-[2-Ethoxycarbonyl-1-phenyl-eth-(E)-ylideneamino]-benzoic acid methyl ester
CAS No.:117874-60-9
Molecular Formula:C₁₉H₁₉NO₄
Molecular Weight:325.364
Hs Code.:

Synonyms:2-[2-Ethoxycarbonyl-1-phenyl-eth-(E)-ylideneamino]-benzoic acid methyl ester

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Chemical Property of 2-[2-Ethoxycarbonyl-1-phenyl-eth-(E)-ylideneamino]-benzoic acid methyl ester

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Technology Process of 2-[2-Ethoxycarbonyl-1-phenyl-eth-(E)-ylideneamino]-benzoic acid methyl ester

There total 1 articles about 2-[2-Ethoxycarbonyl-1-phenyl-eth-(E)-ylideneamino]-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 134-20-3
2-carbomethoxyaniline

: 117874-60-9
2-[2-Ethoxycarbonyl-1-phenyl-eth-(E)-ylideneamino]-benzoic acid methyl ester

Guidance literature:: With methanesulfonic acid; In benzene; for 36h; Heating;
DOI:10.1021/jm00122a018

Reference yield: 35.0%

: 117874-60-9
2-[2-Ethoxycarbonyl-1-phenyl-eth-(E)-ylideneamino]-benzoic acid methyl ester

: 107027-76-9
8-(methoxycarbonyl)-2-phenyl-4(1H)-quinolone

Guidance literature:: In various solvent(s); at 255 ℃;
DOI:10.1021/jm00122a018

Reference yield:

: 117874-60-9
2-[2-Ethoxycarbonyl-1-phenyl-eth-(E)-ylideneamino]-benzoic acid methyl ester

: 107027-06-5
N-<2-(dimethylamino)ethyl>-2-(4-aminophenyl)quinoline-8-carboxamide dihydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: 35 percent / various solvent(s) / 255 °C

2: 98 percent / KOH / aq. ethanol / 2 h / Heating

3: 1.) KOH, Al-foil, 2) HCl, FeCl₃ / 1.) 50percent aq. EtOH, 2.) reflux, 30 min

4: 35 percent / fuming HNO₃ / 2 h / -5 °C

5: 1.) 1,1'-carbonyldiimidazole, 3.) conc. HCl / 1.) DMF, 20 to 40 deg C, 20 min, 2.) 20 deg C, 15 min

6: 72 percent / 1.) Fe-powder, acetic acid, 2.) conc. HCl / aq. ethanol / 1 h / Heating

With hydrogenchloride; potassium hydroxide; nitric acid; iron(III) chloride; iron; acetic acid; 1,1'-carbonyldiimidazole; aluminium; In ethanol;
DOI:10.1021/jm00122a018