2-Chloro-3-[(2,4-dinitro-phenyl)-hydrazono]-butyric acid (E)-3-phenyl-allyl ester

Base Information

Chemical Name:2-Chloro-3-[(2,4-dinitro-phenyl)-hydrazono]-butyric acid (E)-3-phenyl-allyl ester
CAS No.:121721-15-1
Molecular Formula:C₁₉H₁₇ClN₄O₆
Molecular Weight:432.82
Hs Code.:

Synonyms:2-Chloro-3-[(2,4-dinitro-phenyl)-hydrazono]-butyric acid (E)-3-phenyl-allyl ester

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Chemical Property of 2-Chloro-3-[(2,4-dinitro-phenyl)-hydrazono]-butyric acid (E)-3-phenyl-allyl ester

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Technology Process of 2-Chloro-3-[(2,4-dinitro-phenyl)-hydrazono]-butyric acid (E)-3-phenyl-allyl ester

There total 3 articles about 2-Chloro-3-[(2,4-dinitro-phenyl)-hydrazono]-butyric acid (E)-3-phenyl-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 74959-17-4
cinnamyl 2-chloroacetoacetate

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 121721-15-1
2-Chloro-3-[(2,4-dinitro-phenyl)-hydrazono]-butyric acid (E)-3-phenyl-allyl ester

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; for 24h; Ambient temperature;

Reference yield:

: 104-54-1
3-Phenylpropenol

: 121721-15-1
2-Chloro-3-[(2,4-dinitro-phenyl)-hydrazono]-butyric acid (E)-3-phenyl-allyl ester

Guidance literature:: Multi-step reaction with 3 steps

2: 82 percent / sulphuryl chloride / CH₂Cl₂ / 1.) 0 deg C, 15 h, 2.) room temperature, 4 h

3: 74 percent / conc. HCl / tetrahydrofuran / 24 h / Ambient temperature

With hydrogenchloride; sulfuryl dichloride; In tetrahydrofuran; dichloromethane;

Reference yield:

: 61363-91-5
(E)-(3-phenylallyl) 3-oxo-butyrate

: 121721-15-1
2-Chloro-3-[(2,4-dinitro-phenyl)-hydrazono]-butyric acid (E)-3-phenyl-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / sulphuryl chloride / CH₂Cl₂ / 1.) 0 deg C, 15 h, 2.) room temperature, 4 h

2: 74 percent / conc. HCl / tetrahydrofuran / 24 h / Ambient temperature

With hydrogenchloride; sulfuryl dichloride; In tetrahydrofuran; dichloromethane;