(S)-benzyl 2-((tert-butoxycarbonyl)amino)5-((tert-butyldiphenylsilyl)oxy)pentanoate

Base Information

Chemical Name:(S)-benzyl 2-((tert-butoxycarbonyl)amino)5-((tert-butyldiphenylsilyl)oxy)pentanoate
CAS No.:1073554-61-6
Molecular Formula:C₃₃H₄₃NO₅Si
Molecular Weight:561.794
Hs Code.:

Synonyms:(S)-benzyl 2-((tert-butoxycarbonyl)amino)5-((tert-butyldiphenylsilyl)oxy)pentanoate

Suppliers and Price of (S)-benzyl 2-((tert-butoxycarbonyl)amino)5-((tert-butyldiphenylsilyl)oxy)pentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-benzyl 2-((tert-butoxycarbonyl)amino)5-((tert-butyldiphenylsilyl)oxy)pentanoate

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Technology Process of (S)-benzyl 2-((tert-butoxycarbonyl)amino)5-((tert-butyldiphenylsilyl)oxy)pentanoate

There total 2 articles about (S)-benzyl 2-((tert-butoxycarbonyl)amino)5-((tert-butyldiphenylsilyl)oxy)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91229-97-9
(S)-2-[N-(tert-butoxycarbonyl)amino]-5-hydroxypentanoic acid benzyl ester

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1073554-61-6
(S)-benzyl 2-((tert-butoxycarbonyl)amino)5-((tert-butyldiphenylsilyl)oxy)pentanoate

Guidance literature:: With triethylamine; dmap; In N,N-dimethyl-formamide; for 96h;

Reference yield:

: Boc-Glu-OBzl

: 1073554-61-6
(S)-benzyl 2-((tert-butoxycarbonyl)amino)5-((tert-butyldiphenylsilyl)oxy)pentanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 1 h / -15 - -10 °C

1.2: 0.83 h / 0 - 25 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 0.42 h / 20 °C

With 1H-imidazole; chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;