benzyl(2S)-5-{[tert-butyl(diphenyl)silyl]oxy}-2-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}pentanoate

Base Information

Chemical Name:benzyl(2S)-5-{[tert-butyl(diphenyl)silyl]oxy}-2-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}pentanoate
CAS No.:1404089-95-7
Molecular Formula:C₄₃H₄₅NO₅Si
Molecular Weight:683.919
Hs Code.:

Synonyms:benzyl(2S)-5-{[tert-butyl(diphenyl)silyl]oxy}-2-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}pentanoate

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Chemical Property of benzyl(2S)-5-{[tert-butyl(diphenyl)silyl]oxy}-2-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}pentanoate

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Technology Process of benzyl(2S)-5-{[tert-butyl(diphenyl)silyl]oxy}-2-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}pentanoate

There total 6 articles about benzyl(2S)-5-{[tert-butyl(diphenyl)silyl]oxy}-2-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.4%

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: C₂₈H₃₅NO₃Si

: 1404089-95-7
benzyl(2S)-5-{[tert-butyl(diphenyl)silyl]oxy}-2-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}pentanoate

Guidance literature:: With sodium hydrogencarbonate; In water; at 20 ℃; for 0.25h;

Reference yield:

: 122350-52-1
(4S)-5-benzyloxy-4-(9H-fluoren-9-ylmethoxycarbonylamino)-5-oxopentanoic acid

: 1404089-95-7
benzyl(2S)-5-{[tert-butyl(diphenyl)silyl]oxy}-2-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}pentanoate

Guidance literature:: (4S)-5-benzyloxy-4-(9H-fluoren-9-ylmethoxycarbonylamino)-5-oxopentanoic acid; With triethylamine; isobutyl chloroformate; In tetrahydrofuran; at -35 - -30 ℃; for 2h;

With sodium tetrahydroborate; In tetrahydrofuran; at 0 ℃; for 2h;

Reference yield:

: C₂₈H₂₈O₅

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1404089-95-7
benzyl(2S)-5-{[tert-butyl(diphenyl)silyl]oxy}-2-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}pentanoate

Guidance literature:: C₂₈H₂₈O₅; With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

tert-butylchlorodiphenylsilane; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h; Time; Temperature;