carbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P;O,P)ruthenium(II)*0.5hexane

Base Information

Chemical Name:carbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P;O,P)ruthenium(II)*0.5hexane
CAS No.:109011-67-8
Molecular Formula:0C₆H₁₄*C₃₁H₃₄Cl₂O₃P₂Ru
Molecular Weight:731.621
Hs Code.:

Synonyms:carbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P;O,P)ruthenium(II)*0.5hexane

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Chemical Property of carbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P;O,P)ruthenium(II)*0.5hexane

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Technology Process of carbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P;O,P)ruthenium(II)*0.5hexane

There total 2 articles about carbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P;O,P)ruthenium(II)*0.5hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 109011-63-4
trans-dichloro-cis-bis((2-methoxyethyl)diphenylphosphane-O,P)ruthenium(II) * ethanol

: 109011-67-8
carbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P;O,P)ruthenium(II)*0.5hexane

Guidance literature:: With CO; In dichloromethane; CO is introduced to a soln. of Ru-compd. at 0°C for 30 min.; CO is removed with a flowing inert gas, to the soln. n-pentane is added, crystals are filtered off, recrystn. from CH2Cl2/n-hexane, drying at 20°C in vac., elem. anal.;

Reference yield: 82.0%

: 109011-71-4
cis-dicarbonyl-cis-dichloro-trans-bis((2-methoxyethyl)diphenylphosphane-P)ruthenium(II)

: 109011-67-8
carbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P;O,P)ruthenium(II)*0.5hexane

Guidance literature:: With CO; In tetrahydrofuran; Irradiation (UV/VIS); Irradiation of a soln. of Ru-compd. at -20°C for 1h under CO.; CO is removed by flowing Ar or N2 gas, pentane is added to the soln., residue is recrystd. from CH2Cl2/n-hexane and dried in vac. at 20°C elem. anal.;