cis-dicarbonyl-cis-dichloro-trans-bis((2-methoxyethyl)diphenylphosphane-P)ruthenium(II)

Base Information

Chemical Name:cis-dicarbonyl-cis-dichloro-trans-bis((2-methoxyethyl)diphenylphosphane-P)ruthenium(II)
CAS No.:109011-71-4
Molecular Formula:C₃₂H₃₄Cl₂O₄P₂Ru
Molecular Weight:716.543
Hs Code.:

Synonyms:cis-dicarbonyl-cis-dichloro-trans-bis((2-methoxyethyl)diphenylphosphane-P)ruthenium(II)

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Chemical Property of cis-dicarbonyl-cis-dichloro-trans-bis((2-methoxyethyl)diphenylphosphane-P)ruthenium(II)

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Technology Process of cis-dicarbonyl-cis-dichloro-trans-bis((2-methoxyethyl)diphenylphosphane-P)ruthenium(II)

There total 4 articles about cis-dicarbonyl-cis-dichloro-trans-bis((2-methoxyethyl)diphenylphosphane-P)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 14898-67-0
ruthenium(III) chloride trihydrate

: 68899-50-3
(2-methoxyethyl)diphenylphosphine

: 109011-71-4
cis-dicarbonyl-cis-dichloro-trans-bis((2-methoxyethyl)diphenylphosphane-P)ruthenium(II)

Guidance literature:: With CO; In 2-methoxy-ethanol; Through a boiling soln. of RuCl3*3H2O CO is introduced for 5 h, to this mixt. a soln. of ligand-compd. is dropwise added (N2 or Ar).; Cooling to 6°C, elem. anal.;

Reference yield: 83.0%

: carbonyl-cis-dichloro-cis-bis{(2-methoxyethyl)diphenylphosphane-P;O',P'}ruthenium(II)

: 109011-71-4
cis-dicarbonyl-cis-dichloro-trans-bis((2-methoxyethyl)diphenylphosphane-P)ruthenium(II)

Guidance literature:: With carbon monoxide; In toluene; Ar atmosphere; refluxing (24 h, CO); pptn. on addn. of hexane, filtration, washing (hexane), drying (vac., room temp.); elem. anal.;