trans-dichloro-cis-bis((2-methoxyethyl)diphenylphosphane-O,P)ruthenium(II) * ethanol

Base Information

Chemical Name:trans-dichloro-cis-bis((2-methoxyethyl)diphenylphosphane-O,P)ruthenium(II) * ethanol
CAS No.:109011-63-4
Molecular Formula:C₂H₆O*C₃₀H₃₄Cl₂O₂P₂Ru
Molecular Weight:706.591
Hs Code.:

Synonyms:trans-dichloro-cis-bis((2-methoxyethyl)diphenylphosphane-O,P)ruthenium(II) * ethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-dichloro-cis-bis((2-methoxyethyl)diphenylphosphane-O,P)ruthenium(II) * ethanol

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Technology Process of trans-dichloro-cis-bis((2-methoxyethyl)diphenylphosphane-O,P)ruthenium(II) * ethanol

There total 1 articles about trans-dichloro-cis-bis((2-methoxyethyl)diphenylphosphane-O,P)ruthenium(II) * ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 109011-71-4
cis-dicarbonyl-cis-dichloro-trans-bis((2-methoxyethyl)diphenylphosphane-P)ruthenium(II)

: 109011-63-4
trans-dichloro-cis-bis((2-methoxyethyl)diphenylphosphane-O,P)ruthenium(II) * ethanol

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); Irradiation at 35°C for 1 h under introducing of N2 or Ar.; Solvent is removed in vac., residue is taken up in hot ethanol, after cooling to 6°C ppt. is recrystd. from acetone, elem. anal.;

Reference yield: 94.0%

: 109011-63-4
trans-dichloro-cis-bis((2-methoxyethyl)diphenylphosphane-O,P)ruthenium(II) * ethanol

: 109011-67-8
carbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P;O,P)ruthenium(II)*0.5hexane

Guidance literature:: With CO; In dichloromethane; CO is introduced to a soln. of Ru-compd. at 0°C for 30 min.; CO is removed with a flowing inert gas, to the soln. n-pentane is added, crystals are filtered off, recrystn. from CH2Cl2/n-hexane, drying at 20°C in vac., elem. anal.;

Reference yield: 93.0%

: 109011-63-4
trans-dichloro-cis-bis((2-methoxyethyl)diphenylphosphane-O,P)ruthenium(II) * ethanol

: 109063-35-6
trans-dicarbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P)ruthenium(II)

Guidance literature:: With CO; In dichloromethane; CO is introduced to a soln. of Ru-compd. at 0°C for 30 min (Ar or N2).; Pptn. with CO-saturated n-hexane, recrystn. from CH2Cl2/n-hexane under CO below 20°C and dried at 20°C under flowing CO, elem. anal.;