(1R,4S)-4-Methyl-1-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-7-oxabicyclo<2.2.1>hepta-2,5-dien-2,3-dicarbonsaeure-dimethylester

Base Information

Chemical Name:(1R,4S)-4-Methyl-1-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-7-oxabicyclo<2.2.1>hepta-2,5-dien-2,3-dicarbonsaeure-dimethylester
CAS No.:108869-69-8
Molecular Formula:C₄₅H₄₆O₁₀
Molecular Weight:746.854
Hs Code.:

Synonyms:(1R,4S)-4-Methyl-1-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-7-oxabicyclo<2.2.1>hepta-2,5-dien-2,3-dicarbonsaeure-dimethylester

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Chemical Property of (1R,4S)-4-Methyl-1-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-7-oxabicyclo<2.2.1>hepta-2,5-dien-2,3-dicarbonsaeure-dimethylester

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Technology Process of (1R,4S)-4-Methyl-1-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-7-oxabicyclo<2.2.1>hepta-2,5-dien-2,3-dicarbonsaeure-dimethylester

There total 4 articles about (1R,4S)-4-Methyl-1-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-7-oxabicyclo<2.2.1>hepta-2,5-dien-2,3-dicarbonsaeure-dimethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 108869-63-2
5-Methyl-2-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)furan

: 762-42-5
dimethyl acetylenedicarboxylate

: 108943-84-6
(1S,4R)-4-Methyl-1-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-7-oxabicyclo<2.2.1>hepta-2,5-dien-2,3-dicarbonsaeure-dimethylester

: 108869-69-8
(1R,4S)-4-Methyl-1-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-7-oxabicyclo<2.2.1>hepta-2,5-dien-2,3-dicarbonsaeure-dimethylester

Guidance literature:: With hydroquinone; In 1,4-dioxane; at 55 ℃; for 48h; under 4500360 Torr;

Reference yield:

: 534-22-5
2-methylfuran

: 108869-69-8
(1R,4S)-4-Methyl-1-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-7-oxabicyclo<2.2.1>hepta-2,5-dien-2,3-dicarbonsaeure-dimethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / 0.56 M ZnCl₂*OEt₂ / CH₂Cl₂ / 1 h / Ambient temperature

2: 70 percent / hydroquinone / dioxane / 48 h / 55 °C / 4500360 Torr

With zinc chloride diethyl ether; hydroquinone; In 1,4-dioxane; dichloromethane;

Reference yield:

: 74808-09-6
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl trichloroacetimidate

: 108869-69-8
(1R,4S)-4-Methyl-1-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-7-oxabicyclo<2.2.1>hepta-2,5-dien-2,3-dicarbonsaeure-dimethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / 0.56 M ZnCl₂*OEt₂ / CH₂Cl₂ / 1 h / Ambient temperature

2: 70 percent / hydroquinone / dioxane / 48 h / 55 °C / 4500360 Torr

With zinc chloride diethyl ether; hydroquinone; In 1,4-dioxane; dichloromethane;