benzoic acid (1S)-1-methoxycarbonyl-2-phenylethyl ester

Base Information

Chemical Name:benzoic acid (1S)-1-methoxycarbonyl-2-phenylethyl ester
CAS No.:185378-48-7
Molecular Formula:C₁₇H₁₆O₄
Molecular Weight:284.312
Hs Code.:

Synonyms:benzoic acid (1S)-1-methoxycarbonyl-2-phenylethyl ester

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Chemical Property of benzoic acid (1S)-1-methoxycarbonyl-2-phenylethyl ester

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Technology Process of benzoic acid (1S)-1-methoxycarbonyl-2-phenylethyl ester

There total 20 articles about benzoic acid (1S)-1-methoxycarbonyl-2-phenylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 51507-18-7
methyl 2-diazohydrocinnamate

: 65-85-0,8013-63-6
benzoic acid

: (S)-3-methoxy-3-oxo-2-phenylpropyl benzoate

: 185378-48-7
benzoic acid (1S)-1-methoxycarbonyl-2-phenylethyl ester

Guidance literature:: With C₂HF₆NO₄S₂*C₂₇H₃₀BNO; In dichloromethane; at -78 ℃; for 0.5h; Reagent/catalyst; Solvent; enantioselective reaction; Catalytic behavior; Inert atmosphere;
DOI:10.1002/anie.201612655

Reference yield:

: Benzoic acid (E)-1-methoxycarbonyl-2-phenyl-vinyl ester

: 185378-48-7
benzoic acid (1S)-1-methoxycarbonyl-2-phenylethyl ester

Guidance literature:: With (+)-1,2-bis-((2S,5S)-2,5-diethylphospholano)benzene(cyclooctadiene)rhodium(I) trifluoromethanesulfonate; hydrogen; In methanol; for 48h; under 3102.9 Torr; Ambient temperature;
DOI:10.1021/ja974278b

Reference yield:

: 98-88-4
benzoyl chloride

: 185378-48-7
benzoic acid (1S)-1-methoxycarbonyl-2-phenylethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine

2: bis-TMS peroxide; (+)-trans-1,2-bis(tosylamino)cyclohexane; K₂CO₃ / SnCl₄

3: sodium methoxide

With pyridine; bis-trimethylsilanyl peroxide; potassium carbonate; (S,S)-N,N'-bis(p-tolylsulfonyl)-trans-cyclohexane-1,2-diamine; sodium methylate; tin(IV) chloride; 2: Baeyer-Villiger oxidation;
DOI:10.1021/jo051568z