4-cyclohexyl-1,5,6,7-tetrakis(trifluoromethyl)-2,3,4-triazabicyclo<3.2.0>hepta-2.6-diene

Base Information

• Chemical Name: 4-cyclohexyl-1,5,6,7-tetrakis(trifluoromethyl)-2,3,4-triazabicyclo<3.2.0>hepta-2.6-diene
• CAS No.: 73688-06-9
• Molecular Formula: C₁₄H₁₁F₁₂N₃
• Molecular Weight: 449.242

Synonyms:4-cyclohexyl-1,5,6,7-tetrakis(trifluoromethyl)-2,3,4-triazabicyclo<3.2.0>hepta-2.6-diene

Chemical Property of 4-cyclohexyl-1,5,6,7-tetrakis(trifluoromethyl)-2,3,4-triazabicyclo<3.2.0>hepta-2.6-diene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-cyclohexyl-1,5,6,7-tetrakis(trifluoromethyl)-2,3,4-triazabicyclo<3.2.0>hepta-2.6-diene

There total 3 articles about 4-cyclohexyl-1,5,6,7-tetrakis(trifluoromethyl)-2,3,4-triazabicyclo<3.2.0>hepta-2.6-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.9%

8-cyclohexyl-1,2,4,5-tetrakis-trifluoromethyl-(1rH,2tH,4tH,5cH)-3-thia-6,7,8-triaza-tricyclo[3.3.0.02,4]oct-6-ene (64724-55-6) → 4-cyclohexyl-1,5,6,7-tetrakis(trifluoromethyl)-2,3,4-triazabicyclo<3.2.0>hepta-2.6-diene (73688-06-9)

Guidance literature:

With triphenylphosphine; In pentane;

DOI:10.1021/jo01303a009

Reference yield:

1,2,3,4-tetrakis(trifluoromethyl)-5-thiabicyclo{2.1.0}pent-2-ene (39091-73-1) → 4-cyclohexyl-1,5,6,7-tetrakis(trifluoromethyl)-2,3,4-triazabicyclo<3.2.0>hepta-2.6-diene (73688-06-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 80.5 percent / CH₂Cl₂ / 24 h / Ambient temperature; in the dark

2: 83.9 percent / triphenylphosphine / pentane

With triphenylphosphine; In dichloromethane; pentane;

DOI:10.1021/jo01303a009

Reference yield:

cyclohexyl azide (19573-22-9) → 4-cyclohexyl-1,5,6,7-tetrakis(trifluoromethyl)-2,3,4-triazabicyclo<3.2.0>hepta-2.6-diene (73688-06-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 80.5 percent / CH₂Cl₂ / 24 h / Ambient temperature; in the dark

2: 83.9 percent / triphenylphosphine / pentane

With triphenylphosphine; In dichloromethane; pentane;

DOI:10.1021/jo01303a009

upstream raw materials:

8-cyclohexyl-1,2,4,5-tetrakis-trifluoromethyl-(1rH,2tH,4tH,5cH)-3-thia-6,7,8-triaza-tricyclo[3.3.0.0^2,4]oct-6-ene

1,2,3,4-tetrakis(trifluoromethyl)-5-thiabicyclo{2.1.0}pent-2-ene

cyclohexyl azide

Downstream raw materials:

Cyclohexyl-[(Z)-4-diazo-5,5,5-trifluoro-1,2,3-tris-trifluoromethyl-pent-2-en-(Z)-ylidene]-amine

Cyclohexyl-[2,2,2-trifluoro-1-(1,2,3-tris-trifluoromethyl-cycloprop-2-enyl)-eth-(Z)-ylidene]-amine

N-cyclohexyl-2,3,4,5-tetrakis(trifluoromethyl)pyrrole

N-cyclohexyl (Dewar pyrrole)

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 73688-06-9 4-cyclohexyl-1,5,6,7-tetrakis(trifluoromethyl)-2,3,4-triazabicyclo<3.2.0>hepta-2.6-diene

Send

Send

Metric Ton KG G Pound L ML

Send

Send