Technology Process of C30H27F6NO4
There total 5 articles about C30H27F6NO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dimethylsulfide borane complex / tetrahydrofuran / 18 h / 23 °C / Inert atmosphere
1.2: 18 h / 0 - 23 °C / Inert atmosphere
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere
With
oxalyl dichloride; dimethylsulfide borane complex; dimethyl sulfoxide;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: platinum(IV) oxide; hydrogen / ethanol / 48 h / 23 °C
2.1: toluene-4-sulfonic acid / ethanol / 4 h / Reflux
3.1: dimethylsulfide borane complex / tetrahydrofuran / 18 h / 23 °C / Inert atmosphere
3.2: 18 h / 0 - 23 °C / Inert atmosphere
4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere
With
platinum(IV) oxide; oxalyl dichloride; dimethylsulfide borane complex; hydrogen; toluene-4-sulfonic acid; dimethyl sulfoxide;
In
tetrahydrofuran; ethanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: toluene-4-sulfonic acid / ethanol / 4 h / Reflux
2.1: dimethylsulfide borane complex / tetrahydrofuran / 18 h / 23 °C / Inert atmosphere
2.2: 18 h / 0 - 23 °C / Inert atmosphere
3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere
With
oxalyl dichloride; dimethylsulfide borane complex; toluene-4-sulfonic acid; dimethyl sulfoxide;
In
tetrahydrofuran; ethanol; dichloromethane;