(4R,5R)-4,5-di-tert-butyl-1-(2-isopropyl-4-methoxy-5-tert-butylphenyl) imidazolidine

Base Information

• Chemical Name: (4R,5R)-4,5-di-tert-butyl-1-(2-isopropyl-4-methoxy-5-tert-butylphenyl) imidazolidine
• CAS No.: 1224151-47-6
• Molecular Formula: C₂₅H₄₄N₂O
• Molecular Weight: 388.637

Synonyms:(4R,5R)-4,5-di-tert-butyl-1-(2-isopropyl-4-methoxy-5-tert-butylphenyl) imidazolidine

Chemical Property of (4R,5R)-4,5-di-tert-butyl-1-(2-isopropyl-4-methoxy-5-tert-butylphenyl) imidazolidine

Chemical Property:

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Technology Process of (4R,5R)-4,5-di-tert-butyl-1-(2-isopropyl-4-methoxy-5-tert-butylphenyl) imidazolidine

There total 1 articles about (4R,5R)-4,5-di-tert-butyl-1-(2-isopropyl-4-methoxy-5-tert-butylphenyl) imidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + (1R,2R)-1-amino-2-(2-isopropyl-4-methoxy-5-tert-butylbenzenamine)-1,2-di-tertbutylethane (1224151-64-7) → (4R,5R)-4,5-di-tert-butyl-1-(2-isopropyl-4-methoxy-5-tert-butylphenyl) imidazolidine (1224151-47-6)

Guidance literature:

In dichloromethane; at 21 ℃; for 24h; Inert atmosphere;

DOI:10.1002/adsc.200900269

Reference yield: 47.0%

(4R,5R)-4,5-di-tert-butyl-1-(2-isopropyl-4-methoxy-5-tert-butylphenyl) imidazolidine (1224151-47-6) + benzyl bromide (100-39-0) → (4R,5R)-4,5-di-tert-butyl-1-benzyl-3-(2-isopropyl-4-methoxy-5-tert-butylphenyl)imidazolidine (1224151-51-2)

Guidance literature:

With potassium carbonate; In acetone; at 100 ℃; for 24h; sealed tube; Inert atmosphere;

DOI:10.1002/adsc.200900269

Reference yield: 44.0%

(4R,5R)-4,5-di-tert-butyl-1-(2-isopropyl-4-methoxy-5-tert-butylphenyl) imidazolidine (1224151-47-6) + propyl bromide (106-94-5) → (4R,5R)-4,5-di-tert-butyl-1-propyl-3-(2-isopropyl-4-methoxy-5-tert-butylphenyl)imidazolidine (1224151-50-1)

Guidance literature:

With potassium carbonate; In acetone; at 100 ℃; for 24h; sealed tube; Inert atmosphere;

DOI:10.1002/adsc.200900269

upstream raw materials:

formaldehyd

(1R,2R)-1-amino-2-(2-isopropyl-4-methoxy-5-tert-butylbenzenamine)-1,2-di-tertbutylethane

Downstream raw materials:

(4R,5R)-4,5-di-tert-butyl-1-benzyl-3-(2-isopropyl-4-methoxy-5-tert-butylphenyl)imidazolidine

(4R,5R)-4,5-di-tert-butyl-1-propyl-3-(2-isopropyl-4-methoxy-5-tert-butylphenyl)imidazolidine

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