diisopropyl (S)-N₂,N₆-dibenzoyl-9-[3-hydroxy-2-(phosphonomethoxy)propyl]-2,6-diaminopurine

Base Information

• Chemical Name: diisopropyl (S)-N₂,N₆-dibenzoyl-9-[3-hydroxy-2-(phosphonomethoxy)propyl]-2,6-diaminopurine
• CAS No.: 1374997-62-2
• Molecular Formula: C₂₉H₃₅N₆O₇P
• Molecular Weight: 610.607

Synonyms:diisopropyl (S)-N₂,N₆-dibenzoyl-9-[3-hydroxy-2-(phosphonomethoxy)propyl]-2,6-diaminopurine

Chemical Property of diisopropyl (S)-N₂,N₆-dibenzoyl-9-[3-hydroxy-2-(phosphonomethoxy)propyl]-2,6-diaminopurine

Chemical Property:

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Technology Process of diisopropyl (S)-N₂,N₆-dibenzoyl-9-[3-hydroxy-2-(phosphonomethoxy)propyl]-2,6-diaminopurine

There total 1 articles about diisopropyl (S)-N₂,N₆-dibenzoyl-9-[3-hydroxy-2-(phosphonomethoxy)propyl]-2,6-diaminopurine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

diisopropyl {[(1S)-2-(2,6-diamino-9H-purin-9-yl)-1-(hydroxymethyl)ethyl]oxy}methylphosphonate (1374997-60-0) + benzoyl chloride (98-88-4) → diisopropyl (S)-N2,N6-dibenzoyl-9-[3-hydroxy-2-(phosphonomethoxy)propyl]-2,6-diaminopurine (1374997-62-2)

Guidance literature:

diisopropyl {[(1S)-2-(2,6-diamino-9H-purin-9-yl)-1-(hydroxymethyl)ethyl]oxy}methylphosphonate; With pyridine; trimethylsilyl bromide; for 0.5h;

benzoyl chloride; at 20 ℃; for 2h;

With ammonia; In water; at 20 ℃; for 0.5h;

DOI:10.1016/j.tet.2012.03.066

Reference yield: 80.0%

diisopropyl (S)-N2,N6-dibenzoyl-9-[3-hydroxy-2-(phosphonomethoxy)propyl]-2,6-diaminopurine (1374997-62-2) → (S)-3-(N2,N6-dibenzoyl-2,6-diamino-9H-purin-9-yl)-2-[(diisopropylphosphono)methoxy]propanoic acid (1389321-44-1)

Guidance literature:

With sodium hypochlorite; sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In acetonitrile; at 20 ℃; for 24h; pH=6.7; aq. phosphate buffer;

DOI:10.1016/j.tet.2012.03.066

upstream raw materials:

diisopropyl {[(1S)-2-(2,6-diamino-9H-purin-9-yl)-1-(hydroxymethyl)ethyl]oxy}methylphosphonate

benzoyl chloride

Downstream raw materials:

(S)-3-(N₂,N₆-dibenzoyl-2,6-diamino-9H-purin-9-yl)-2-[(diisopropylphosphono)methoxy]propanoic acid

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