[Pd(κ2-C6H4N(Me)CH2Ph-2)I(PPh3)]

Base Information

Chemical Name:[Pd(κ2-C6H4N(Me)CH2Ph-2)I(PPh3)]
CAS No.:677027-13-3
Molecular Formula:C₃₂H₂₉INPPd
Molecular Weight:691.887
Hs Code.:

Synonyms:[Pd(κ2-C6H4N(Me)CH2Ph-2)I(PPh3)]

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Chemical Property of [Pd(κ2-C6H4N(Me)CH2Ph-2)I(PPh3)]

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Technology Process of [Pd(κ2-C6H4N(Me)CH2Ph-2)I(PPh3)]

There total 2 articles about [Pd(κ2-C6H4N(Me)CH2Ph-2)I(PPh3)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: tris(dibenzylideneacetone)dipalladium ⁽⁰⁾

: 677027-04-2
N-benzyl-2-iodo-N-methylaniline

: 603-35-0
triphenylphosphine

: 677027-13-3
[Pd(κ2-C6H4N(Me)CH2Ph-2)I(PPh3)]

Guidance literature:: In benzene; (Ar); addn. of palladium complex and phosphine to a soln. of ligand in benzene, stirring at room temp. for 3 d; evapn., chromy. (SiO2, hexane to CH2Cl2), crystn. (hexane/ethyl acetate); elem. anal.;
DOI:10.1021/om034270c

Reference yield: 63.0%

: 677027-15-5
trans-[Pd(C₆H₄N(Me)CH₂Ph-2)I(PPh₃)2]

: 677027-13-3
[Pd(κ2-C6H4N(Me)CH2Ph-2)I(PPh3)]

: 677027-08-6
[Pd(κ2-C6H4N(Me)CH2Ph-2)OH(PPh3)]

Guidance literature:: With SiO₂; In hexane; ethyl acetate; (Ar); flash chromy. (SiO2, hexane to hexane/ethyl acetate 1:1);
DOI:10.1021/om034270c

Reference yield: 64.0%

: 67-66-3,8013-54-5
chloroform

: 677027-13-3
[Pd(κ2-C6H4N(Me)CH2Ph-2)I(PPh3)]

: 7732-18-5
water

: 141-78-6
ethyl acetate

: [Pd(κ2-C(O)C6H4N(Me)CH2Ph-2)I(PPh3)]*0.5EtOAc

Guidance literature:: With (CH₃)3COK; In chloroform; tert-butyl alcohol; (Ar); addn. of a soln. of potassium salt in tert-butyl alcohol, keeping for 5 min at room temp., addn. of a soln. of palladium complex in CHCl3 dropwise, stirring at room temp. for 5 h; evapn., chromy. (SiO2, hexane to hexane/ethyl acetate 1:1), crystn. (ethyl acetate); elem. anal.;
DOI:10.1021/om034270c