[3-(4-bromophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-bromophenyl)-5-phenylpyrrol-2-ylidene]amine

Base Information

• Chemical Name: [3-(4-bromophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-bromophenyl)-5-phenylpyrrol-2-ylidene]amine
• CAS No.: 603105-63-1
• Molecular Formula: C₃₂H₂₁Br₂N₃
• Molecular Weight: 607.347

Synonyms:[3-(4-bromophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-bromophenyl)-5-phenylpyrrol-2-ylidene]amine

Chemical Property of [3-(4-bromophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-bromophenyl)-5-phenylpyrrol-2-ylidene]amine

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Technology Process of [3-(4-bromophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-bromophenyl)-5-phenylpyrrol-2-ylidene]amine

There total 4 articles about [3-(4-bromophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-bromophenyl)-5-phenylpyrrol-2-ylidene]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

3-(4-bromophenyl)-4-nitro-1-phenylbutan-1-one (219607-51-9) → [3-(4-bromophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-bromophenyl)-5-phenylpyrrol-2-ylidene]amine (603105-63-1)

Guidance literature:

With ammonium acetate; In butan-1-ol; for 56h; Inert atmosphere; Reflux;

DOI:10.1021/ol102701v

Reference yield:

4-bromo-benzaldehyde (1122-91-4) → [3-(4-bromophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-bromophenyl)-5-phenylpyrrol-2-ylidene]amine (603105-63-1)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hydroxide / ethanol / 20 °C

2: diethylamine / methanol / Reflux

3: ammonium acetate / butan-1-ol / 56 h / Inert atmosphere; Reflux

With ammonium acetate; diethylamine; potassium hydroxide; In methanol; ethanol; butan-1-ol;

DOI:10.1021/ol102701v

Reference yield:

acetophenone (98-86-2) → [3-(4-bromophenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-bromophenyl)-5-phenylpyrrol-2-ylidene]amine (603105-63-1)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hydroxide / ethanol / 20 °C

2: diethylamine / methanol / Reflux

3: ammonium acetate / butan-1-ol / 56 h / Inert atmosphere; Reflux

With ammonium acetate; diethylamine; potassium hydroxide; In methanol; ethanol; butan-1-ol;

DOI:10.1021/ol102701v

upstream raw materials:

3-(4-bromophenyl)-1-phenylprop-2-en-1-one

4-bromo-benzaldehyde

acetophenone

3-(4-bromophenyl)-4-nitro-1-phenylbutan-1-one

Downstream raw materials:

C₈₆H₈₅N₅O₄

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