C₃₃H₃₉NO₆

Base Information

• Chemical Name: C₃₃H₃₉NO₆
• CAS No.: 1308271-88-6
• Molecular Formula: C₃₃H₃₉NO₆
• Molecular Weight: 545.676
• Mol file: 1308271-88-6.mol

Synonyms:C₃₃H₃₉NO₆

Chemical Property of C₃₃H₃₉NO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₃H₃₉NO₆

There total 10 articles about C₃₃H₃₉NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C31H35NO6 (1276112-29-8) + vinylmagnesium chloride (3536-96-7) → C33H39NO6 (1308271-88-6)

Guidance literature:

In tetrahydrofuran; at -78 ℃; for 1.5h;

DOI:10.1016/j.tetlet.2011.01.018

Reference yield:

C27H27NO5 (1308271-84-2) → C33H39NO6 (1308271-88-6)

Guidance literature:

Multi-step reaction with 5 steps

1: sodium tetrahydroborate / methanol / 24 h / 0 - 20 °C

2: silver(l) oxide / N,N-dimethyl-formamide / 24 h / 20 °C

3: ammonium cerium (IV) nitrate / water; acetonitrile / 2.5 h / 0 - 20 °C

4: dmap; triethylamine / dichloromethane / 2 h / 0 °C

5: tetrahydrofuran / 1.5 h / -78 °C

With dmap; sodium tetrahydroborate; ammonium cerium (IV) nitrate; triethylamine; silver(l) oxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1016/j.tetlet.2011.01.018

Reference yield:

C34H35NO5 (1276112-28-7) → C33H39NO6 (1308271-88-6)

Guidance literature:

Multi-step reaction with 3 steps

1: ammonium cerium (IV) nitrate / water; acetonitrile / 2.5 h / 0 - 20 °C

2: dmap; triethylamine / dichloromethane / 2 h / 0 °C

3: tetrahydrofuran / 1.5 h / -78 °C

With dmap; ammonium cerium (IV) nitrate; triethylamine; In tetrahydrofuran; dichloromethane; water; acetonitrile;

DOI:10.1016/j.tetlet.2011.01.018

upstream raw materials:

C₂₇H₂₇NO₅

C₂₇H₂₉NO₅

C₃₄H₃₅NO₅

C₂₆H₂₇NO₄

Downstream raw materials:

C₃₃H₄₁NO₆

C₃₆H₄₅NO₈

C₃₃H₄₁NO₅

C₃₂H₃₉NO₆