N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methylphenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide

Base Information

Chemical Name:N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methylphenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide
CAS No.:330940-83-5
Molecular Formula:C₂₄H₂₂ClN₅O₂
Molecular Weight:447.924
Hs Code.:

Synonyms:N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methylphenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide

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Chemical Property of N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methylphenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide

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Technology Process of N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methylphenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide

There total 6 articles about N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methylphenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methylphenyl}(4-cyanophenyl)carboxamide

: 109-81-9
N-methyl-ethane-1,2-diamine

: 330940-83-5
N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methylphenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide

Guidance literature:: N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methylphenyl}(4-cyanophenyl)carboxamide; With hydrogenchloride; In methanol; ethyl acetate; at 0 - 20 ℃;

N-methyl-ethane-1,2-diamine; In methanol; for 2h; Reflux;

Reference yield:

: 3113-72-2
5-methyl-2-nitrobenzoic acid

: 330940-83-5
N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methylphenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

1.2: 20 °C

2.1: hydrogen; platinum on carbon / methanol / 2 h / 20 °C

3.1: pyridine / dichloromethane / 20 °C

4.1: hydrogenchloride / ethyl acetate; methanol / 0 - 20 °C

4.2: 2 h / Reflux

With pyridine; hydrogenchloride; oxalyl dichloride; platinum on carbon; hydrogen; N,N-dimethyl-formamide; In methanol; dichloromethane; ethyl acetate;

Reference yield:

: 280773-04-8
N-(5-chloro(pyridin-2-yl))(5-methyl-2-nitrophenyl)carboxamide

: 330940-83-5
N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methylphenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen; platinum on carbon / methanol / 2 h / 20 °C

2.1: pyridine / dichloromethane / 20 °C

3.1: hydrogenchloride / ethyl acetate; methanol / 0 - 20 °C

3.2: 2 h / Reflux

With pyridine; hydrogenchloride; platinum on carbon; hydrogen; In methanol; dichloromethane; ethyl acetate;