Dimethyl phenyl phosphorotetrathioate

Base Information

• Chemical Name: Dimethyl phenyl phosphorotetrathioate
• CAS No.: 93449-40-2
• Molecular Formula: C₈H₁₁PS₄
• Molecular Weight: 266.413
• DSSTox Substance ID: DTXSID201285409
• Mol file: 93449-40-2.mol

Synonyms:Dimethyl phenyl phosphorotetrathioate;DTXSID201285409;93449-40-2

Chemical Property of Dimethyl phenyl phosphorotetrathioate

Chemical Property:

• XLogP3: 4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 265.94812204
• Heavy Atom Count: 13
• Complexity: 181

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CSP(=S)(SC)SC1=CC=CC=C1

Technology Process of Dimethyl phenyl phosphorotetrathioate

There total 5 articles about Dimethyl phenyl phosphorotetrathioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl phenyl disulfide (14173-25-2) → trimethyl tetrathiophosphate (2386-38-1) + triphenyl thiophosphite (1095-04-1) + Tetrathiophosphoric acid methyl ester diphenyl ester (93449-41-3) + Tetrathiophosphoric acid dimethyl ester phenyl ester (93449-40-2)

Guidance literature:

With tetraphosphorus trisulfide; at 60 ℃; for 1h; Irradiation;

DOI:10.1039/DT9840001517

Reference yield:

methyl phenyl disulfide (14173-25-2) → triphenyl thiophosphite (1095-04-1) + Tetrathiophosphoric acid methyl ester diphenyl ester (93449-41-3) + Tetrathiophosphoric acid dimethyl ester phenyl ester (93449-40-2) + C13H13PS3 (93449-39-9)

Guidance literature:

With tetraphosphorus trisulfide; at 60 ℃; for 1h; Further byproducts given; Irradiation;

DOI:10.1039/DT9840001517

Reference yield:

diphenyldisulfane (882-33-7) → Tetrathiophosphoric acid dimethyl ester phenyl ester (93449-40-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Irradiation

2: 39 percent Spectr_. / P₄S₃ / 1 h / 60 °C / Irradiation

With tetraphosphorus trisulfide;

DOI:10.1039/DT9840001517

upstream raw materials:

methyl phenyl disulfide

Dimethyldisulphide

diphenyldisulfane