[2-(4-benzyloxy-phenyl)-5,5-dimethyl-1-oxy-5H-imidazol-4-yl]-dimethyl-amine

Base Information

• Chemical Name: [2-(4-benzyloxy-phenyl)-5,5-dimethyl-1-oxy-5H-imidazol-4-yl]-dimethyl-amine
• CAS No.: 1027932-18-8
• Molecular Formula: C₂₀H₂₃N₃O₂
• Molecular Weight: 337.422

Synonyms:[2-(4-benzyloxy-phenyl)-5,5-dimethyl-1-oxy-5H-imidazol-4-yl]-dimethyl-amine

Chemical Property of [2-(4-benzyloxy-phenyl)-5,5-dimethyl-1-oxy-5H-imidazol-4-yl]-dimethyl-amine

Chemical Property:

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Technology Process of [2-(4-benzyloxy-phenyl)-5,5-dimethyl-1-oxy-5H-imidazol-4-yl]-dimethyl-amine

There total 5 articles about [2-(4-benzyloxy-phenyl)-5,5-dimethyl-1-oxy-5H-imidazol-4-yl]-dimethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-(4-benzyloxy-phenyl)-5,5-dimethyl-1-oxy-5H-imidazole-4-carbonitrile (1026915-72-9) + dimethyl amine (124-40-3) → [2-(4-benzyloxy-phenyl)-5,5-dimethyl-1-oxy-5H-imidazol-4-yl]-dimethyl-amine (1027932-18-8)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1039/b418707e

Reference yield:

2-(4-benzyloxy-phenyl)-4,5,5-trimethyl-2,5-dihydro-imidazol-1-ol (851705-73-2) → [2-(4-benzyloxy-phenyl)-5,5-dimethyl-1-oxy-5H-imidazol-4-yl]-dimethyl-amine (1027932-18-8)

Guidance literature:

Multi-step reaction with 4 steps

1: 90 percent / PbO₂ / CH₂Cl₂

2: 80 percent / i-Pr-ONa; isopropyl nitrite / propan-2-ol / 20 °C

3: 90 percent / TsCl; Et₃N / CHCl₃ / 1 h

4: 90 percent / CH₂Cl₂ / 20 °C

With i-propyl nitrite; sodium isopropylate; lead dioxide; triethylamine; p-toluenesulfonyl chloride; In dichloromethane; chloroform; isopropyl alcohol;

DOI:10.1039/b418707e

Reference yield:

2-(4-benzyloxy-phenyl)-4,4,5-trimethyl-4H-imidazole 3-oxide (1026926-68-0) → [2-(4-benzyloxy-phenyl)-5,5-dimethyl-1-oxy-5H-imidazol-4-yl]-dimethyl-amine (1027932-18-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 80 percent / i-Pr-ONa; isopropyl nitrite / propan-2-ol / 20 °C

2: 90 percent / TsCl; Et₃N / CHCl₃ / 1 h

3: 90 percent / CH₂Cl₂ / 20 °C

With i-propyl nitrite; sodium isopropylate; triethylamine; p-toluenesulfonyl chloride; In dichloromethane; chloroform; isopropyl alcohol;

DOI:10.1039/b418707e

upstream raw materials:

2-(4-benzyloxy-phenyl)-5,5-dimethyl-1-oxy-5H-imidazole-4-carbonitrile

dimethyl amine

2-(4-benzyloxy-phenyl)-4,5,5-trimethyl-2,5-dihydro-imidazol-1-ol

2-(4-benzyloxy-phenyl)-4,4,5-trimethyl-4H-imidazole 3-oxide

Downstream raw materials:

C₂₂H₂₈N₃O₂

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