allyl (2S,4R)-4-(bis(tert-butoxycarbonyl)amino)-2-methyl-5-phenylpentanoate

Base Information

Chemical Name:allyl (2S,4R)-4-(bis(tert-butoxycarbonyl)amino)-2-methyl-5-phenylpentanoate
CAS No.:936691-39-3
Molecular Formula:C₂₅H₃₇NO₆
Molecular Weight:447.572
Hs Code.:

Synonyms:allyl (2S,4R)-4-(bis(tert-butoxycarbonyl)amino)-2-methyl-5-phenylpentanoate

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Chemical Property of allyl (2S,4R)-4-(bis(tert-butoxycarbonyl)amino)-2-methyl-5-phenylpentanoate

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Technology Process of allyl (2S,4R)-4-(bis(tert-butoxycarbonyl)amino)-2-methyl-5-phenylpentanoate

There total 6 articles about allyl (2S,4R)-4-(bis(tert-butoxycarbonyl)amino)-2-methyl-5-phenylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₈H₅₃NO₅Si

: 936691-39-3
allyl (2S,4R)-4-(bis(tert-butoxycarbonyl)amino)-2-methyl-5-phenylpentanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 0.44 g / tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

2: Dess-Martin periodinane / CH₂Cl₂ / 20 °C

3: 0.68 g / 2-methyl-2-butene; sodium chlorite; sodium dihydrogen phosphate monohydrate / 2-methyl-propan-2-ol; H₂O; tetrahydrofuran / 20 °C

4: 0.36 g / cesium carbonate / dimethylformamide

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; tetrabutyl ammonium fluoride; caesium carbonate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ol070415q

Reference yield:

: 936691-38-2
di(tert-butyl) (2R,4S)-5-hydroxy-4-methyl-1-phenylpentan-2-yliminodicarbonate

: 936691-39-3
allyl (2S,4R)-4-(bis(tert-butoxycarbonyl)amino)-2-methyl-5-phenylpentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: Dess-Martin periodinane / CH₂Cl₂ / 20 °C

2: 0.68 g / 2-methyl-2-butene; sodium chlorite; sodium dihydrogen phosphate monohydrate / 2-methyl-propan-2-ol; H₂O; tetrahydrofuran / 20 °C

3: 0.36 g / cesium carbonate / dimethylformamide

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; caesium carbonate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ol070415q

Reference yield:

: C₂₂H₃₃NO₅

: 936691-39-3
allyl (2S,4R)-4-(bis(tert-butoxycarbonyl)amino)-2-methyl-5-phenylpentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 0.68 g / 2-methyl-2-butene; sodium chlorite; sodium dihydrogen phosphate monohydrate / 2-methyl-propan-2-ol; H₂O; tetrahydrofuran / 20 °C

2: 0.36 g / cesium carbonate / dimethylformamide

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; caesium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ol070415q