N-((E)-1-(4-chlorophenyl)-3-phenylallylidene)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-((E)-1-(4-chlorophenyl)-3-phenylallylidene)-4-methylbenzenesulfonamide
CAS No.:1380402-84-5
Molecular Formula:C₂₂H₁₈ClNO₂S
Molecular Weight:395.909
Hs Code.:

Synonyms:N-((E)-1-(4-chlorophenyl)-3-phenylallylidene)-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((E)-1-(4-chlorophenyl)-3-phenylallylidene)-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of N-((E)-1-(4-chlorophenyl)-3-phenylallylidene)-4-methylbenzenesulfonamide

There total 1 articles about N-((E)-1-(4-chlorophenyl)-3-phenylallylidene)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 22966-22-9
(E)-1-(4-chlorophenyl)-3-phenyl-2-propen-1-one

: 70-55-3
toluene-4-sulfonamide

: 1380402-84-5
N-((E)-1-(4-chlorophenyl)-3-phenylallylidene)-4-methylbenzenesulfonamide

Guidance literature:: With titanium tetrachloride; triethylamine; In dichloromethane; at 0 ℃; for 16h; Reflux; Inert atmosphere;
DOI:10.1002/anie.201109061

Reference yield:

: 1380402-84-5
N-((E)-1-(4-chlorophenyl)-3-phenylallylidene)-4-methylbenzenesulfonamide

: 864658-42-4
2,2-dimethylpropanoicphenylacetic anhydride

: 1380402-70-9
(3R,4R)-6-(4-chlorophenyl)-3,4-diphenyl-1-tosyl-3,4-dihydropyridin-2(1H)-one

: 6-(4-chlorophenyl)-3,4-diphenyl-1-tosyl-3,4-dihydropyridin-2(1H)-one

Guidance literature:: With (R)-(+)-2-phenyl-2,3-dihydrobenzo[d]imidazo[2,1-b]thiazole; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 20 ℃; for 2h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201109061

Reference yield:

: 1380402-84-5
N-((E)-1-(4-chlorophenyl)-3-phenylallylidene)-4-methylbenzenesulfonamide

: 108-59-8
malonic acid dimethyl ester

: dimethyl 2-[(S,E)-3-(4-chlorophenyl)-1-phenyl-3-(tosylamino)allyl]malonate

: dimethyl 2-[(S,Z)-3-(4-chlorophenyl)-1-phenyl-3-(tosylamino)allyl]malonate

: dimethyl 2-[(R,E)-3-(4-chlorophenyl)-1-phenyl-3-(tosylamino)allyl]malonate

: dimethyl 2-[(R,Z)-3-(4-chlorophenyl)-1-phenyl-3-(tosylamino)allyl]malonate

Guidance literature:: With lanthanum(lll) triflate; (S,S)-2,6-bis(4-phenyl-2-oxazolinyl)pyridine; In dichloromethane; at 20 ℃; for 24h; Overall yield = 80%; Inert atmosphere; Schlenk technique; Molecular sieve;
DOI:10.1002/chem.201302687